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희석제량에 따른 탄탈륨 분말 특성 및 반응온도의 영향 KCI 등재

Characteristic of Tantalum Powder and Effect of Reaction Temperature on the amount of Diluent

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Pure tantalum powder has been produced by combining Na as a reducing agent, as feed material, KCl and KF as a diluent in a stainless steel(SUS) bomb, using the method of metallothermic reduction. The present study investigated the effect of the amount of the diluent and reaction temperature on the characteristics of tantalum powder in the production process. The temperature applied in this study and the amount of the additional reductant from +5% of the theoretical amount used for the reduction of the entire . The results showed that as the amount of the diluent increased, the reaction temperature became lower because the diluent prevented a temperature rise. Also, according to the mixture ratio of the feed materials and the diluent changed from 1 : 0.25 to 1 : 2, the particle size decreased from to and a particle size distribution which is below 325 mesh in fined powder increases from 71% to 83%. The average size of Tantalum powder, , was close to that of the commercial powders(). Also under this condition, impurities contained in the powder were within the range allowed for the commercial Ta powders.

저자
  • 윤재식
  • 박형호
  • 배인성
  • 정성만
  • 김병일