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Production of B‑doped reduced graphene oxide using wet‑process in tetrahydrofuran KCI 등재

  • 언어ENG
  • URLhttps://db.koreascholar.com/Article/Detail/420674
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Carbon Letters (Carbon letters)
한국탄소학회 (Korean Carbon Society)
초록

Graphene-based materials show excellent properties in various applications because of their electrical properties, large surface areas, and high tolerance for chemical modification. The use of wet-process is a promising way for their mass production. Heteroatom doping is one of the common methods to improve their electrical, physical, and electrochemical properties. In this work, we develop a new route for the production B-doped graphene-based materials using low-temperature wet-process, which is the reaction between graphene oxide suspensions and a BH3 adduct in tetrahydrofuran under reflux. Elemental mapping images show well-dispersed B atoms along the materials. Various spectroscopic characterizations confirm the reduction of the graphene oxide and incorporation of B atoms into the carbon network as high as ~ 2 at%. The materials showed electrocatalytic activity for oxygen reduction reactions.

목차
    Abstract
    1 Introduction
    2 Experimental
        2.1 Preparation of graphite oxide
        2.2 Preparation of B-rG-O samples
        2.3 Electrochemical measurements
        2.4 Instruments
    3 Results and discussion
        3.1 Characterizations of materials
        3.2 Electrochemical properties of the materials
    4 Conclusions
    Acknowledgements 
    References
저자
  • Yunseok Shin(Department of Chemistry and Chemical Engineering, Inha University)
  • Sungjin Park(Department of Chemistry and Chemical Engineering, Inha University)