논문 상세보기

Fe-Cr-Al 기 산화물 분산강화 합금의 미세조직에 미치는 분말제조 공정 영향 KCI 등재 SCOPUS

Effect of Powder Synthesis Method on the Microstructure of Oxide Dispersion Strengthened Fe-Cr-Al Based Alloys

  • 언어KOR
  • URLhttps://db.koreascholar.com/Article/Detail/331051
구독 기관 인증 시 무료 이용이 가능합니다. 4,000원
한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

An optimum route to fabricate oxide dispersion strengthened ferritic superalloy with desired microstructure was investigated. Two methods of high energy ball milling or polymeric additive solution route for developing a uniform dispersion of Y2O3 particles in Fe-Cr-Al-Ti alloy powders were compared on the basis of the resulting microstructures. Microstructural observation revealed that the crystalline size of Fe decreased with increases in milling time, to values of about 15-20 nm, and that an FeCr alloy phase was formed. SEM and TEM analyses of the alloy powders fabricated by solution route using yttrium nitrate and polyvinyl alcohol showed that the nano-sized Y-oxide particles were well distributed in the Fe based alloy powders. The prepared powders were sintered at 1000 and 1100 oC for 30 min in vacuum. The sintered specimen with heat treatment before spark plasma sintering at 1100 oC showed a more homogeneous microstructure. In the case of sintering at 1100 oC, the alloys exhibited densified microstructure and the formation of large reaction phases due to oxidation of Al.

목차
1. 서 론
 2. 실험 방법
 3. 결과 및 고찰
 4. 결 론
 Acknowledgement
 References
저자
  • 박성현(서울과학기술대학교 신소재공학과) | Sung Hyun Park (Department of Materials Science and Engineering, Seoul National University of Science and Technology, Seoul 01811, Republic of Korea)
  • 오승탁†(서울과학기술대학교 신소재공학과) | Sung-Tag Oh† (Department of Materials Science and Engineering, Seoul National University of Science and Technology, Seoul 01811, Republic of Korea) Corresponding author