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타이타늄 합금 분말의 열적산화를 통한 TiO2 나노와이어의 합성 KCI 등재

Synthesis of TiO2 Nanowires by Thermal Oxidation of Titanium Alloy Powder

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

One-dimensional rutile TiO2 is an important inorganic compound with applicability in sensors, solar cells, and Li-based batteries. However, conventional synthesis methods for TiO2 nanowires are complicated and entail risks of environmental contamination. In this work, we report the growth of TiO2 nanowires on a Ti alloy powder (Ti-6wt%Al- 4wt%V, Ti64) using simple thermal oxidation under a limited supply of O2. The optimum condition for TiO2 nanowire synthesis is studied for variables including temperature, time, and pressure. TiO2 nanowires of ~5 μm in length and 100 nm in thickness are richly synthesized under the optimum condition with single-crystalline rutile phases. The formation of TiO2 nanowires is greatly influenced by synthesis temperature and pressure. The synthesized TiO2 nanowires are characterized using field-emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD), and high-resolution transmission electron microscopy (HR-TEM).

목차
Abstract
 1. 서 론
 2. 실험 방법
 3. 결과 및 고찰
 4. 결 론
 감사의 글
 References
저자
  • 김유영(경남과학기술대학교 기계공학과) | Yoo-Young Kim
  • 조권구(경상대학교 나노신소재융합공학과 & 그린에너지 융합연구소) | Kwon-Koo Cho Corresponding Author