An aluminum powder compact consolidated by a powder-in sheath rolling (PSR) method was severely deformed by accumulative roll-bonding (ARB) process. The ARB process was performed up to 8 cycles at ambient temperature without lubrication. Optical microscope and transmission electron microscope observations revealed that microstructure of the ARB-processed Al powder compact is inhomogeneous in the thickness direction. The ultra-fine subgrains often reported in the ARB-processed bulky materials were also developed near surface of the Al powder compacts in this study. Tensile strength of the ARB-processed Al powder compact increased at the 1st cycle, but from the 2nd cycle it rather decreased slightly.

Aluminum based metal matrix composite reinforced with SiC particles was fabricated by the powder-in sheath rolling method. A stainless steel tube with outer diameter of 12 mm and wall thickness of 1mm was used as a sheath. Mixture of aluminum powder and SiC particles of which volume content was varied from 5 to 20vol.% was filled in the tube by tap filling and then rolled to 75% reduction at ambient temperature. The rolled specimen was sintered at 56 for 0.5hr. The tensile strength of the (SiC)/Al composite increased with the volume content of SiC particles, and at 20vol.% it reached a maximum of 100㎫ which is 1.6 times higher than unreinforced material. The elongation decreased with the volume content of O particles. The mechanical properties of the (SiC)/Al composite fabricated by the powder-in sheath rolling is compared with that of (AlO)/Al composite by the same process.ess.

Recently, it has been found that mechanical alloying (MA) facilitates the nanocomposites formation of metal-metal oxide systems through solid-state reduction during ball milling. In this work, we studied the MA effect of FeO-M (M = Al, Ti) systems, where pure metals are used as reducing agents. It is found that composite powders in which O and TiO are dispersed in -Fe matrix with nano-sized grains are obtained by mechanical alloying of FeO with Al and Ti for 25 and 75 hours, respectively. It is suggested that the large negative heat associated with the chemical reduction of magnetite by aluminum is responsible for the shorter MA time for composite powder formation in FeO-Al system. X-ray diffraction results show that the reduction of magnetite by Al and Ti if a relatively simple reaction, involving one intermediate phase of FeAlO or FeTiO. The average grain size of -Fe in Fe-TiO composite powders is in the range of 30 nm. From magnetic measurement, we can also obtain indirect information about the details of the solid-state reduction process during MA.

Mechanical alloying (MA) by high energy ball mill of Pure chromium Powders was carried out under the nitrogen gas atmosphere. Cr-N amorphous alloy powders have been produced through the solid-gas reaction subjected to MA. The atomic structure during amorphization process was observed by X-ray and neutron diffractions. An advantage of the neutron diffraction technique allows us to observe the local atomic structure surrounding a nitrogen atom. The coordination number of metal atoms around a N atom turns out to be 5.5 atoms. This implies that a nitrogen atom is located at both of centers of the tetrahedron and octahedron formed by metal atoms to stabilize an amorphous Cr-N structure. Also, we have revealed that a Cr-N amorphous alloy may produced from a mixture of pure Cr and Cr nitrides powders by solid-solid reaction during mechanical alloying.

The composites fabricated by powder in sheath rolling method were cold-rolled by 50% reduction and annealed for 1.8 ks at various temperatures ranging from 200 to 50, for improvement of the mechanical properties. The mechanical properties and texture of the composites after rolling and annealing were investigated. The tensile strength of the composites increased significantly due to work hardening after cold rolling, however it decreased due to restoration after annealing. The strength of the composites was improved by thermo mechanical treatment. On the other hand, the texture evolution with annealing temperatures wa,i different between the unreinforced material and the composites. The unreinforced material showed a deformation (rolling) texture of which main component is ｛112｝<111> at annealing temperatures up to 30. However, the composites have already exhibited a recrystallization texture of which main component is ｛001｝<100> after annealing at 20. This proves that the critical temperature for recrystailization is lower in the composites than in the unreinforced ones.

본 논문에서는 균열을 지닌 축대칭 문제를 해석하기 위하여 시간적분형 운동방정식을 바탕으로 한 유한요소 해법을 제시한다. 유한요소메쉬는 8절점 등매개변수 사변형 요소와 균열선단에서의 1/4절점 삼각형 특이요소로 구성되며, 동적 응력확대계수는 균열면상의 1/4절점의 y방향 변위로부터 구한다. 제시된 해법의 정확성과 타당성을 검증하기 위하여 내부에 원환균열을 지닌 무한 탄성체가 균열면상에서 충격하중을 받을 때의 동적 응력확대계수를 계산하고 타 수치결과와 비교 검토하였다. 응용 예제로서 원환균열과 원주균열을 지닌 중실축과 중공축의 동적 응력확대계수를 균열의 길이와 축의 길이에 따른 영향을 자세히 조사하였다. 균열길이가 커지면 동적 응력확대계수가 커지고, 축의 길이가 길어지면 동적 응력확대계수 곡선의 폭도 함께 증가됨을 확인하였다. 그리고 균열의 위치가 안쪽에 포함될 경우보다는 바깥쪽에 포함될 때 더 큰 동적 응력확대계수가 발생됨을 밝힌다.

Aluminum-based composites were fabricated by a powder-in sheath rolling method. A stainless steel tube with outer diameter of 12 mm and wall thickness of 1 mm was used as a sheath. A mixture of aluminum powder and particles of which volume content was varied from 5 to 20%, was filled in the tube by tap filling and then rolled by 75% reduction in thickness at ambient temperature. The rolled specimen was then sintered at 56 for 0.5 h. The mixture of Al powders and particles was successfully consolidated by the sheath rolling. The composite fabricated by the sheath rolling showed a recrystallized structure, while unreinforced Al powder compact fabricated by the same procedure showed a deformed structure. The unreinforced Al powder compact was characterized by a deformation (rolling) texture of which main component is {112}<111>, while the composite showed a mixed texture oi deformation and recrystallization. The sintering resulted in recrystallization in Al powder compact and grain growth in the composite.

The powder-in sheath rolling was applied to the fabrication of composite. A stainless steel tube with outer diameter of 12 mm and wall thickness of 1 mm was used as a sheath. Mixture of aluminum powder and particles of which volume content was varied from 5 to 20 vol.% was filled in the tube by tap filling and then rolled to 75% reduction at ambient temperature. The re]]ed specimen was sintered at 56 for 0.5 hr. The composite fabricated by the sheath rolling and subsequent sintering showed the relative density higher than 0.96. The tensile strength of the composite increased with the volume content of particles, and it reached a maximum of 90 MPa which is 1.5 times higher than unreinforced material. The elongation decreased with the volume content of particles. It is concluded that the powder-in sheath rolling is an effective method for fabrication of composite.

Lee et al. reported that a mixture of Cu and Ta, the combination of which is characterized by a positive heat of mixing, of +2 kJ/㏖, can be amorphized by mechanical alloying(MA). It is our aim to investigate to what extent the MA is capable of producing a non-equilibrium phase with increasing the heat of mixing. The system chosen is the binary with =+19 kJ/㏖. The mechanical alloying was carried out using a Fritsch P-5 planetary mill under Ar gas atmosphere. The vial and balls are made of Cu containing 1.8-2.0 wt.%Be to avoid contaminations arising mainly from Fe when steel balls and vial are used. The MA powders were characterized by the X-ray diffraction, EXAFS and thermal analysis. We conclude that two phase mixture of nanocrystalline fcc-Cu and bcc-Mo with grain size of 10 nm is formed by the ball-milling for a 3:7 mixture of pure Cu and Mo, the evidence for which has been deduced from the thermodynamic and structural analysis based on the DSC, X-ray diffraction and EXAFS spectra.

본 논문에서는 축방향 압축하중을 받는 다퐁간분리된 적층 보-기둥의 자유진동과 좌팔에 대한 해석을 수행하였다. 다층간분리된 적층 보-기둥의 고유진동수와 탄성 좌굴 하중에 대한 층간분리의 영향을 조사하기 위해 층간분리의 양단에서 기울기와 곡률이 일정하다는 가정을 적용하여 일반적인 운동학적 연속 조건을 유도하였다. 전체 다층간분리된 보-기둥을 부분으로 분할하고, 연속조건에 따른 반복관계를 각 하부 보-기둥에 부과함으로써 다층간분리된 보-기둥의 특성방정식을 구하였다. 축방향 증분 압축 하중에 따른 다층간분리된 보-기둥의 고유진동수와 탄성 좌굴 하중을 구하였으며 이는 손상되지 않은 적층 보-기둥의 최대 탄성 좌굴 하중에 한정된다 연구를 통하여 층간분리의 크기, 위치, 수가 고유진동수와 특히 탄성 좌굴 하중에 큰 영향을 미치는 것을 알 수 있었다.

현재 기계적 합금화법에서는 주로 합금을 구성하는 성분원소 분말을 불활성분위기에서 볼밀처리 함으로써 함금화를 시키거나 모합금에 산화물을 분산시켜 복합화시키는 공정을 통하여 각종 화합물, 비정질상 및 과포화고용체등의 준안정상의 합성 뿐만이 아니라 초미세조직의 생성에 관한 폭 넓은 분야의 연구가 행하여지고 있다. 한편 MA에서는 볼멀처리중 기계적 에너지의 투여에 의하여 실제 반응온도보다 낮은 온도에서 발생하는 특이한 화학반응 즉 Mechanochemical

A nitrogen gas atomized aluminum powder was consolidated by powder-in sheath rolling method. A pure aluminum tube with outer diameter of 12 mm and wall thickness of 1mm was used as a sheath. The aluminum tube filled with the aluminum powder, first, was cold-rolled to the thickness of 6mm for performing, and then consolidated by the cold rolling and/or subsequent hot rolling at 360, 460 and . The aluminum powder compact fabricated by the sheath rolling showed high relative density more than 0.96 at any rolling conditions. The 0.2% proof stress increased with increasing hot rolling reduction and hot rolling temperature. Tensile strength was hardly affected by change in the hot rolling reduction, whereas it decreased with increasing hot rolling temperature. The powder compact showed the large elongation when cold rolling or hot rolling reduction was large. It was found that the sheath rolling was an effective method for consolidation of aluminum powder.