역세척이 가능한 평막형 분리막 모듈을 분리막 생물반응기(MBR)에 침지시켜 운전 시간에 따른 흡입 압력을 측 정하였다. MLSS 8,000 mg/L 활성 슬러지 수용액에 공칭 세공크기가 0.2 μm, 유효막면적이 128 cm2인 분리막 모듈을 침지 시킨 후 투과 유속, quorum qeunching (QQ) 비드를 변화하며 흡입 압력을 확인하였다. Vacant bead (VB), BH4와 DKY-1의 실험군에서 FR과 SFCO 운전방식에 따른 효과를 비교, 분석하였다. 투과 유속 40 L/m2⋅h 이고 DKY-1 QQ 비드를 주입할 경우 흡입 압력 감소는 가장 효과적이었다. 또한 역세척에 의한 흡입 압력 감소 효과는 DKY-1 QQ 비드의 경우보다 2배 이 상 높게 나타났다.

In liquid scintillation counting, sample radioactivity is analyzed by measuring photons emitted from counting vials. Quenching effect lowers photon intensity from samples, which leads to lower counting efficiency. So an appropriate quenching correction according to characteristics of samples is important. In this study, the quenching correction for H-3 analysis was conducted according to the characteristics of paper packaging material leached samples. The leached samples are made from H-3 leaching method which is in the process of development for H-3 contamination screening. There are several ways of quenching correction such as internal standard (IS) method, quench correction curve and triple-to-double coincidence ratio (TDCR) method, etc. For quench correction curve, quenched standard set, which has the same matrix as experimental samples, is needed to be prepared. Each leached sample, however, has different matrix and color depending on condition of leaching experiment, which means that it is not capable of preparing standard set having same matrix with the samples. In this study, the counting samples are used for plotting quench correction curve instead of quenched standard set. Spectral quench parameter of the external standard [SQP(E)] is used as quench indicating parameter (QIP). TDCR and counting efficiencies determined by IS method are used as counting efficiencies. The quench curve of TDCR versus SQP(E) has R2 = 0.55 and the curve of efficiency from IS method versus SQP(E) has R2 = 0.99. TDCR is known for approximate counting efficiency, however, TDCR as counting efficiency needs careful use for H-3 analysis of leached samples. The curve used efficiency from IS method is suitable for H-3 analysis of leached samples. In this study, the quench correction curve is prepared for H-3 analysis of leached samples of paper packaging material. SQP(E), TDCR and efficiency from IS method was used as parameters to plot the quench correction curve, and, the efficiency from IS method is suitable for H-3 analysis of the leached samples. The result of this study can be used for H-3 analysis of leached samples of paper packaging material.

Al-Cr-Si ternary quench ribbons are fabricated using a single roll method and investigated for their structural and thermal properties. In particular, the sinterability is examined by pulse current sintering to obtain the following results. The Al74Cr20Si6 composition becomes a quasicrystalline single phase; by reducing the amount of Cr, it becomes a twophase mixed structure of Al phase and quasicrystalline phase. As a result of sintering of Al74Cr20Si6, Al77Cr13Si10 and Al90Cr6Si4 compositions, the sintering density is increased with the large amount of Al phase; the sintering density is the highest in Al90Cr6Si4 composition. In addition, as a result of investigating the effects of sintering temperature and pressurization on the sintered density of Al90Cr6Si4, a sintered compact of 99% or more at 513 K and 500 MPa is produced. In particular, since the Al-Cr-Si ternary crystal is more thermally stable than the Al-Cr binary quaternary crystal, it is possible to increase the sintering temperature by about 100 K. Therefore, using an alloy of Al90Cr6Si4 composition, a sintered compact having a sintered density of 99 % or more at 613 K and 250 MPa can be manufactured. It is possible to increase the sintering temperature by using the alloy system as a ternary system. As a result, it is possible to produce a sintered body with higher density than that possible using the binary system, and at half the pressure compared with the conventional Al-Cr binary system.

Direct water quenching technique can be used in hot stamping process to obtain higher cooling rate compared to that of the normal die cooling method. In the direct water quenching process, setting proper water flow rate in consideration of material thickness and the size of the area directly cooled in the component is important to ensure uniform microstructure and mechanical properties. In this study, to derive proper water flow rate conditions that can achieve uniform microstructure and mechanical properties, microstructure and hardness distribution in various water flow rate conditions are measured for 3.2 mm thick boron steel sheet. Hardness distribution is uniform under the flow condition of 1.5 L/min or higher. However, due to the lower cooling rate in that area, the lower flow conditions result in a drastic decrease in hardness in some areas in the hot-stamped part, resulting in low martensite fraction. From these results, it is found that the selection of proper water flow rate is an important factor in hot stamping with direct water quenching process to ensure uniform mechanical properties.

In this study, the direct water quenching technique is applied to validate the applicability of direct water quenching as a cooling method in the hot stamping process of 3.2 mm thick boron steel sheet. Cooling performance of conventional die quenching and direct water quenching is compared. Higher cooling rate is obtained by hot stamping with direct water quenching compared to die quenching. As the flow rate of cooling water increases, the cooling rate increases, and a high cooling rate of 71 oC/s is achieved under flow rate conditions of 0.8 L/min. Through direct water quenching, the cooling time required for sufficient cooling of the sheet is reduced. Full martensitic microstructure is obtained under flow rate condition of 0.8 L/min. Hardness increases with increasing flow rate. From these results, it is verified that the direct water quenching is applicable to the hot stamping of thick boron steel sheet.

Lead free (1-x)(0.675BiFeO3-0.325BaTiO3)- xLiTaO3 (BFBTLT, x = 0, 0.01, 0.02, and 0.03, with 0.6 mol% MnO2 and 0.4 mol% CuO) were prepared by a solid state reaction method, followed by air quenching and their crystalline phase, morphology, dielectric, ferroelectric and piezoelectric properties were explored. An X-ray diffraction study indicates that lithium (Li) and tantalum (Ta) were fully incorporated in the BFBT materials with the absence of any secondary phases. Dense ceramic samples (> 92 %) with a wide range of grain sizes from 3.70 μm to 1.82 μm were obtained in the selected compositions (0 ≤ x ≤ 0.03) of BFBTLT system. The maximum temperatures (Tmax) were mostly higher than 420 oC in the studied composition range. The maximum values of maximum polarization (Pmax ≈ 31.01 μC/cm2), remnant polarization (Prem ≈ 22.82 μC/cm2) and static piezoelectric constant (d33 ≈ 145 pC/N) were obtained at BFBT-0.01LT composition with 0.6 mol% MnO2 and 0.4 mol% CuO. This study demonstrates that the high Tmax and d33 for BFBTLT ceramics are favorable for industrial applications.