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열화학적 방법에 의한 전극용 나노 Cu/Al2O3 복합분말 합성 KCI 등재

Synthesis of Cu/Al2O3 Nanostructured Composite Powders for Electrode Application by Thermochemical Process

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Nanostructured Cu-AlO composite powders were synthesized by thermochemical process. The synthesis procedures are 1) preparation of precursor powder by spray drying of solution made from water-soluble copper and aluminum nitrates, 2) air heat treatments to evaporate volatile components in the precursor powder and synthesis of nano-structured CuO + O, and 3) CuO reduction by hydrogen into pure Cu. The suggested procedures stimulated the formation of the gamma-AlO, and different alumina formation behaviors appeared with various heat treating temperatures. The mean particle size of the final Cu/AlO composite powders produced was 20 nm, and the electrical conductivity and hardness in the hot-extruded bulk were competitive with Cu/AlO composite by the conventional internal oxidation process

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