This study was carried out to suggest a realtime evaluation system for the odor adsorption efficiency with electrochemical sensors. As the results of the experiments for the realtime evaluation system, the correlation coefficient between the sensor signals and the hydrogen sulfide concentration was relatively good, 0.9920 and 0.8340, respectively. The relative standard deviation of three replicative experiments for the adsorption amount in the conditions of 0.5 g and 1.0 g of adsorbent was 6.97% and 3.49%, respectively. This study would contribute the realtime evaluation of odor control efficiency to overcome the limitations of olfactory method and instrumental analysis in terms of cost and technology.