This research is related to the process of refining the raw material, industrial 2-propanone to the 2-propanone of the electronic grade. With this view, the high purity of 2-propanone was obtained through the complex preprocessing(physical adsorption method), distillation process and membrane-filtration of distillate. Impurities were identified by GC and UV, and then we assayed the water content in 2-propanone passing adsorption step made of activated carbon and Zeolite 4A. Furthermore, the distillation was performed with the packed column distillation apparatus to eliminate impurities such as acetaldehyde. Particulates were removed by reduced-pressure filtration through 0.5μm membrane filter and the number of the particulates was measured by particulate counter to confirm the removal of impure particles.