This study evaluated the concentration(OU/m3) of a complex odor being discharged from tire, feedstuff, bakery, paper, casting and painting manufacturing process, correlation between odor concentration(OU/m3) and the odor sensor was investigated. 4 type(A, B, C, D) gas sensors of metal oxide compounds are used in this study. Each odor sample of manufacturing process is diluted with odorless air and diluted odor samples were prepared for five different concentrations. Correlation results(R) of odor sample of tire, feedstuff, bakery, paper manufacturing process ware 0.86~0.99, and odor sample of casting, painting manufacturing process ware more than 0.93. Thus the odor concentration(OU/m3) evaluation by odor sensor was to determine the possible. In particular odor sensor B and D are likely to be effective for evaluation of odor concentration. However, odor samples before evaluation is needed the calibration process depending on the field odor sample to field apply.