In this study, a liquid carbonation method was applied for producing precipitate calcium carbonate by liquid-liquid reaction. We recycled the recycling water of ready-mixed concrete, one of construction waste for use source of carbonate ion. A supernatant separated from the recycling water of ready-mixed concrete, as a result of ICP analysis of a cation, Ca²+ was contained up to 1100 ppm. We used MEA as a CO₂ absorbent for the liquid carbonation. A precipitate CaCO₃ was produced at more than MEA 20 wt%. The precipitate CaCO₃ as a final product was separated and dried. The result of XRD was confirmed the generation of CaCO₃ to calcite structure.