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GC-FID 분석을 이용한 휘발성 유기규소화합물 혼합가스의 검량특성 KCI 등재

Calibration Characteristics of Gaseous Mixtures of Volatile Organic Silicon Compounds on Gas Chromatography with Flame Ionization Detector

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한국폐기물자원순환학회지 (Journal of Korea Society of Waste Management)
한국폐기물자원순환학회 (Korea Society Of Waste Management)
초록

This study assessed the analysis method for measuring volatile organic silicon compounds (namely as siloxanes) by usinggas chromatography with flame ionization detector. Calibration standard gas was made in a laboratory by using six volatileorganic silicons as model gas. Two different types of working gas were prepared to evaluate quality control in GC-FIDanalysis. Less than 0.2 RSD% of repeatability of retention time was observed in the analysis of calibration standard gas. Inthe linearity test, the highest coefficient of determination (R2) was found to be 0.997 for L2 among volatile organic siliconcompounds. This study demonstrated that quantification of volatile organic silicon compounds can be performed by usingGC-FID analysis with direct injection mode, and the GC calibration can be covered by the gas-phase standard method.

저자
  • 이성우(서울과학기술대학교 환경공학과) | Seongwoo Lee
  • 윤승준(한국환경산업기술원) | Seung-Joon Yoon
  • 김대근(서울과학기술대학교 환경공학과) | Daekeun Kim Corresponding author