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pp.55-60
In this study, Ti powder was fabricated from Ti scrap by a hydrogenation-dehydrogenation (HDH)method. The Ti powders were compacted by Spark plasma sintering (SPS) and the microstructure andmechanical properties of the powders were investigated. A hydrogenation reaction of Ti scrap occurred attemperatures near 450oC with a sudden increase in the reaction temperature and a decrease in the pressureof the hydrogen gas as measured in a furnace during the hydrogenation process. In addition, a dehydrogenationprocess was carried out at 750oC for 2hrs in a vacuum of 10-4torr. The Ti powder sizes obtained byhydrogenation-dehydrogenation and mechanical milling processes were in the range of 1~90µm and 1~100µm,respectively. To fabricate Ti compacts, Ti powders were sintered under an applied uniaxial punch pressure of40 MPa at in a range of 900~1200oC for 5 min. The relative density of a SPSed compact was 99.6% at 1100oC,and the tensile strength decreased with an increase in the sintering temperature. However, the hardnessincreased as the sintering temperature increased.
