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기공형성제 PMMA와 WO3 분말 성형체의 열처리를 이용한 W 다공체 제조 KCI 등재

Fabrication of Porous W by Heat Treatment of Pore Forming Agent of PMMA and WO3 Powder Compacts

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Porous W with controlled pore structure was fabricated by thermal decomposition and hydrogen reduction process of PMMA beads and WO3 powder compacts. The PMMA sizes of 8 and 50 μm were used as pore forming agent for fabricating the porous W. The WO3 powder compacts with 20 and 70 vol% PMMA were prepared by uniaxial pressing and sintered for 2 h at 1200oC in hydrogen atmosphere. TGA analysis revealed that the PMMA was decomposed at about 400oC and WO3 was reduced to metallic W at 800oC. Large pores in the sintered specimens were formed by thermal decomposition of spherical PMMA, and their size was increased with increase in PMMA size and the amount of PMMA addition. Also the pore shape was changed from spherical to irregular form with increasing PMMA contents due to the agglomeration of PMMA in the powder mixing process.

목차
Abstract
 1. 서 론
 2. 실험방법
 3. 실험결과 및 고찰
 4. 결 론
 감사의 글
 References
저자
  • 전기철(서울과학기술대학교 신소재공학과) | Ki Cheol Jeon
  • 김영도(한양대학교 신소재공학부) | Young Do Kim
  • 석명진(강원대학교 재료금속공학과) | Myung-Jin Suk
  • 오승탁(서울과학기술대학교 신소재공학과) | Sung-Tag Oh Corresponding author