In this study, ternary compound Max Phase Ti2AlC material was mixed by 3D ball milling as a function of ball milling time. More than 99.5 wt% pure Ti2AlC was synthesized by using spark plasma sintering method at 1000, 1100, 1200, and 1300oC for 60 min. The material characteristics of synthesized samples were examined with relative density, hardness, and electrical conductivity as a function of sintering temperature. The phase composition of bulk was identified by X-ray diffraction. On the basis of FE-SEM result, a terraced structures which consists of several laminated layers were observed. And Ti2AlC bulk material obtained a vickers hardness of 5.1 GPa at the sintering temperature of 1100oC.