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Synthesis and Characterization of ZnAl2O4 Nanopowders by a Reverse Micelle Processing KCI 등재 SCOPUS

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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

Using reverse micelle processing, ZnAl2O4 nanopowders were synthesized from a mixed precursor(consisting of Zn(NO3)2 and Al(NO3)3). The ZnAl2O4 was prepared by mixing the aqueous solution at a molar ratio of Zn : Al = 1 : 2. The average size and distribution of the synthesized powders with heat treatment at 600 oC for 2 h were in the range of 10-20 nm and narrow, respectively. The average size of the synthesized powders increased with increasing water to surfactant molar ratio. The XRD diffraction patterns show that the phase of ZnAl2O4 was spinel(JCPDS No. 05-0669). The synthesized and calcined powders were characterized using a thermogravimetric - differential scanning calorimeter(TG-DSC), X-ray diffraction analysis (XRD), and high resolution transmission electron microscopy(HRTEM). The effects of the synthesis parameter, such as the molar ratio of water to surfactant, are discussed.

목차
1. Introduction
2. Experiment
3. Results and Discussion
4. Conclusions
Acknowledgment
References
저자
  • Son-Jung Hoon(Department of Advanced Materials Science and Engineering, Changwon National University, Gyeongnam 641-773, Korea)
  • Jeongho Sohn(School of Port and Logistics, Kaya University, #208, Samgyero, Gimhae, Gyeongnam 621-748, Korea)
  • Hyung-Sup Shin(Department of Optometry, Kaya University, #208, Samgyero, Gimhae, Gyeongnam 621-748, Korea)
  • Dong-Sik Bae(Department of Advanced Materials Science and Engineering, Changwon National University, Gyeongnam 641-773, Korea) Corresponding Author