논문 상세보기

폴리올 공정과 액상 환원 공정에 따른 은 입자 제조 및 특성 평가 KCI 등재

Fabrication and Characterization of Ag Particles by Polyol Process and Wet Chemical Process

  • 언어KOR
  • URLhttps://db.koreascholar.com/Article/Detail/316687
구독 기관 인증 시 무료 이용이 가능합니다. 4,000원
한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Ag nanoparticles are extensively studied and utilized due to their excellent catalysis, antibiosis and optical properties. They can be easily synthesized by chemical reduction methods and it is possible to prepare particles of uniform size and high purity. These methods are divided into vapor methods and liquid phase reduction methods. In the present study, Ag particles are prepared and analyzed through two chemical reduction methods using solvents containing a silver nitrate precursor. When Ag ions are reduced using a reductant in the aqueous solution, it is possible to control the Ag particle size by controlling the formic acid ratio. In addition, in the Polyol process, Ag nanoparticles prepared at various temperatures and reaction time conditions have multiple twinned and anisotropic structures, and the particle size variation can be confirmed using field emissions scanning electron microscopy and by analyzing the UV-vis spectrum.

목차
1. 서 론
 2. 실험방법
  2.1. Formic acid 액상환원법을 이용한 은 입자 합성
  2.2. 폴리올(Polyol) 공정을 이용한 은 입자 합성
  2.3. 특성평가
 3. 실험결과 및 토론
  3.1. Formic acid 액상환원법을 이용한 은 입자 합성
  3.2. 폴리올(Polyol) 공정을 이용한 은 입자 합성
 4. 결 론
 감사의 글
 References
저자
  • 유주연(단국대학교 에너지공학) | Juyeon Yoo
  • 장효성(단국대학교 에너지공학과) | Hyosung Jang
  • 이근재(단국대학교 에너지공학과) | Kun-Jae Lee Corresponding Author