In this study, we investigated variations in particle size distribution in the process flow from a fluff-SRF manufacturing process in Y city via particle size analysis of waste. About 110 kg of MSW was analyzed in accordance with the process flows for the analysis of the particle size distribution by separating from 300 mm to 10 mm. The first tranche of waste was crushed with a primary crusher such that 100% of particles were smaller than 200 mm. A secondary crusher was used to ensure that 90% of particles were smaller than 10 mm. The crushing function and disintegration effect resulted in waste that contained 30% particles smaller than 10 mm. The primary multistage bulk selection process separated the first non-combustibles from waste passed by the secondary crusher. It produced 19.24% non-combustibles. Secondary multistage bulk selection discharges the final set of non-combustibles from the first non-combustibles after recovering any remaining combustibles. The combustible recovery ratio was 28.24%, and the final non-combustible discharge ratio was about 71.76%. The regular and high-speed disintegrators exhibited 85% and 97% efficiency in producing waste smaller than then 50 mm, respectively. This is thought to improve the yield and quality of SRF in the context of a reasonable management plan via characteristic analysis of residues from the disintegration process.