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이트리아 안정화 지르코니아 나노 분말 합성 KCI 등재 SCOPUS

Hydrothermal Synthesis of 6mol% Yttria Stabilized Cubic ZrO2 Nano Powders

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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

YSZ (Yttria-stabilized zirconia) is a ceramic material that is used for electronic and structural materials due to its excellent mechanical properties and specific electrical characteristics according to the Yttrium addition. Hydrothermal synthesis has several advantages such as fine particle size, uniform crystalline phase, fast reaction time, low process temperature and good dispersion condition. In order to synthesize YSZ nanoparticles with high crystallinity, hydrothermal synthesis was performed at various concentrations of NaOH. The hydrothermal process was held at a low temperature (100 °C), with a short process time (2,4,8 hours); the acidity or alkalinity of solution was controlled in a range of pH 2~12 by addition of NaOH. The optimum condition was found to be pH 12, at which high solubility levels of Y(OH) and Zr(OH) were reported. The synthesized nano powder showed high crystallinity and homogenous composition, and uniform particle size of about 10 nm.

저자
  • 이재훈(경남대학교 메카트로닉스공학과) | Jae-Hoon Lee (Department of Mechatronics Engineering, Kyungnam University, 7 Kyungnamdaehak-ro, Masanhappo-gu, Changwon-si 51767, Republic of Korea)
  • 배성환(경남대학교 나노신소재공학과) | Sung-Hwan Bae (Department of Nano Science and Engineering, Kyungnam University, 7 Kyungnamdaehak-ro, Masanhappo-gu, Changwon-si 51767, Republic of Korea) Corresponding author