논문 상세보기

CuO-Al2O3/camphene 슬러리의 동결건조 공정에 의한 Al2O3 입자분산 Cu 다공체 제조 KCI 등재

Fabrication of Al2O3 Dispersed Porous Cu by Freeze Drying of CuO-Al2O3/Camphene Slurry

  • 언어KOR
  • URLhttps://db.koreascholar.com/Article/Detail/343773
구독 기관 인증 시 무료 이용이 가능합니다. 4,000원
한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Porous Cu with a dispersion of nanoscale Al2O3 particles is fabricated by freeze-drying CuO-Al2O3/camphene slurry and sintering. Camphene slurries with CuO-Al2O3 contents of 5 and 10 vol% are unidirectionally frozen at -30oC, and pores are generated in the frozen specimens by camphene sublimation during air drying. The green bodies are sintered for 1 h at 700oC and 800oC in H2 atmosphere. The sintered samples show large pores of 100 μm in average size aligned parallel to the camphene growth direction. The internal walls of the large pores feature relatively small pores of ~10 μm in size. The size of the large pores decreases with increasing CuO-Al2O3 content by the changing degree of powder rearrangement in the slurry. The size of the small pores decreases with increasing sintering temperature. Microstructural analysis reveals that 100-nm Al2O3 particles are homogeneously dispersed in the Cu matrix. These results suggest that a porous composite body with aligned large pores could be fabricated by a freeze-drying and H2 reducing process.

목차
Abstract
 1. 서 론
 2. 실험 방법
 3. 실험결과 및 고찰
 4. 결 론
 감사의 글
 References
저자
  • 강현지(서울과학기술대학교 신소재공학과) | Hyunji Kang
  • 류도형(서울과학기술대학교 신소재공학과) | Doh-Hyung Riu
  • 오승탁(서울과학기술대학교 신소재공학과) | Sung-Tag Oh Corresponding Author