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Determination of Simultaneous Analytical Method of Residual Pesticides by Gas Chromatography

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한국환경과학회지 (Journal of Environmental Science International)
한국환경과학회 (The Korean Environmental Sciences Society)
초록

The simultaneous determination of residual pesticides was developed using a gas chromatography. In this study, a simple and reliable methodology was improved to detect 175 kinds of residual pesticides by a liquid-liquid extraction procedure, followed by chromatographic analysis by gas chromatography. The 175 kinds of residual pesticides was classified into 4 groups according to the chemical structure, column type, resolution and sensitivity. The soybean sample selected for recovery experiment was not detected any pesticides. The recovery rates were ranged from 70.6% to 119.7% in most pesticides. The relative standard deviation (RSD 0.3~5.6%) was lower than 5.6% in all cases. The limits of detection (LOD) was lower than the maximum residue levels established by Korean legislations. The method has been successfully applied to the analysis of approximately 130 real samples.

목차
Abstract
 1. 서 론
 2. 재료 및 방법
  2.1. 실험재료 및 시약
  2.2. 실험 방법
 3. 결과 및 고찰
  3.1. 농약 성분의 유형별 분류
  3.2. 농약 표준품의 동시다성분 분석
  3.3. Florisil chromatography에서 용매별 정제 효과
  3.4. 대두의 농약성분 회수율
  3.5. 유통농산물에 대한 잔류농약 모니터링
 4. 결 론
 참 고 문 헌
저자
  • 최원조(부산지방식품의약품안전청) | Won Jo Choi (Busan Regional Food & Drug Administration)
  • 최계선(식품의약품안전청) | Gye-Sun Choi (Korea Food & Drug Admonistration)
  • 이희정(부산지방식품의약품안전청) | Hee Jung Lee (Busan Regional Food & Drug Administration)
  • 원영준(식품의약품안전청) | Young Jun Won (Korea Food & Drug Admonistration)
  • 박흥재(인제대학교 환경공학부) | Heung-Jai Park (Department of Environmental Science, Inje University)
  • 김우성(부산지방식품의약품안전청) | Woo Seong Kim (Busan Regional Food & Drug Administration) Corresponding Author