논문 상세보기

고체상미량분석법(SPME)을 이용한 GC/FID에서 PCE 및 TCE 최적 분석법 KCI 등재

The Optimal Analytical Method for the Determination of PCE and TCE by GC/FID with SPME technieque

  • 언어KOR
  • URLhttps://db.koreascholar.com/Article/Detail/363332
서비스가 종료되어 열람이 제한될 수 있습니다.
한국환경과학회지 (Journal of Environmental Science International)
한국환경과학회 (The Korean Environmental Sciences Society)
초록

A new method based on solid phase microextraction(SPME), coupled with GC/FID, has been developed for the determination of PCE and TCE in water samples. The experimental parameters affecting the SPME process (i.e, kinds of fibers, extraction time, desorption time, extraction temperature, volume ratio of sample to headspace, salt addition, and magnetic stirring) were optimized. The coefficients of determination (R2) for PCE and TCE were 0.9951 and 0.9831, respectively when analytes concentration ranges from 10 to 300㎍/L. The relative standard deviations were 3.4 and 2.1% for concentration of 10㎍/L(n=5), respectively. The detection limits of PCE and TCE were 0.5 and 1.3㎍/L, respectively.

저자
  • 안상우(경기대학교 환경공학과) | Sang-Woo Ahn
  • 이시진(경기대학교 환경공학과) | Si-Jin Lee
  • 장순웅(경기대학교 환경공학과) | Soon-Woong Chang Corresponding Author