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Microstructure and Morphology of Titanium Thin Films Deposited by Using Shadow Effect

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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

In order to observe the microstructure and morphology of porous titanium -oxide thin film, deposition is performed under a higher Ar gas pressure than is used in the general titanium thin film production method. Black titanium thin film is deposited on stainless steel wire and Cu thin plate at a pressure of about 12 Pa, but lustrous thin film is deposited at lower pressure. The black titanium thin film has a larger apparent thickness than that of the glossy thin film. As a result of scanning electron microscope observation, it is seen that the black thin film has an extremely porous structure and consists of a separated column with periodic step differences on the sides. In this configuration, due to the shadowing effect, the nuclei formed on the substrate periodically grow to form a step. The surface area of the black thin film on the Cu thin plate changes with the bias potential. It has been found that the bias of the small negative is effective in increasing the surface area of the black titanium thin film. These results suggest that porous titanium-oxide thin film can be fabricated by applying the appropriate oxidation process to black titanium thin film composed of separated columns.

목차
Abstract
1. 서 론
2. 실험 방법
3. 결과 및 고찰
    3.1 Ti 박막의 구조와 색
    3.2 이온충격의 영향
    3.3 박막표면의 결정성장 형태
    3.4 주상결정 측면에 주기적인 요철(凹凸)이 형성된이유
4. 결 론
References
저자
  • 한창석(호서대학교 자동차ICT공학과) | Chang-Suk Han (Dept. of ICT Automotive Engineering, Hoseo University) Corresponding author
  • 진성윤(호서대학교 자동차ICT공학과) | Sung-Yooun Jin (Dept. of ICT Automotive Engineering, Hoseo University)
  • 권혁구(호서대학교 환경공학과) | Hyuk-Ku Kwon (Dept. of Environmental Engineering, Hoseo University)