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용매열 공정을 이용한 세리아(CeO2) 나노분말의 합성 및 분산거동 KCI 등재 SCOPUS

Synthesis and Dispersion of Ceria(CeO2) Nanoparticles by Solvothermal Process

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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

CeO2 nanoparticles, employed in a lot of fields due to their excellent oxidation and reduction properties, are synthesized through a solvothermal process, and a high specific surface area is shown by controlling, among various process parameters in the solvothermal process, the type of solvent. The synthesized CeO2 nanoparticles are about 11~13 nm in the crystallite size and their specific surface area is about 65.38~84.65 m2/g, depending on the amount of ethanol contained in the solvent for the solvothermal process; all synthesized CeO2 nanoparticles shows a fluorite structure. The dispersibility and microstructure of the synthesized CeO2 nanoparticles are investigated according to the species of dispersant and the pH value of the solution; an improvement in dispersibility is shown with the addition of dispersants and control of the pH. Various dispersing properties appear according to the dispersant species and pH in the solution with the synthesized CeO2 nanoparticles, indicating that improved dispersing properties in the synthesized CeO2 nanoparticles can be secured by applying dispersant and pH control simultaneously.

목차
Abstract
1.서 론
2. 실험 방법
    2.1 용매열 공정을 이용한 세리아 나노 분말 합성
    2.2 세리아 나노 분말 분산
3. 결과 및 고찰
    3.1 용매열 공정을 이용한 세리아 나노 분말 합성
    3.2 세리아 나노 분말의 분산 특성
4. 결 론
References
저자
  • 임태섭(창원대학교 신소재공학과) | Tae Seop Lim (School of Nano & Advanced Materials Eng., Changwon National Univ)
  • 옥지영(창원대학교 신소재공학과) | Ji Young Ock (School of Nano & Advanced Materials Eng., Changwon National Univ)
  • 최연빈(창원대학교 신소재공학과) | Yeon Bin Choi (School of Nano & Advanced Materials Eng., Changwon National Univ)
  • 김봉구(창원대학교 신소재공학과) | Bong Gu Kim (School of Nano & Advanced Materials Eng., Changwon National Univ)
  • 손정훈(창원대학교 신소재공학과) | Jeong Hun Son (School of Nano & Advanced Materials Eng., Changwon National Univ)
  • 정연길(창원대학교 신소재공학과) | Yeon Gil Jung (School of Nano & Advanced Materials Eng., Changwon National Univ) Corresponding author