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Y2O3 첨가 탄소 프리폼에 Si 용융 침투에 의해 제조한 반응 소결 탄화규소 KCI 등재

RBSC Prepared by Si Melt Infiltration into the Y2O3 Added Carbon Preform

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

The conversion of carbon preforms to dense SiC by liquid infiltration is a prospectively low-cost and reliable method of forming SiC-Si composites with complex shapes and high densities. Si powder was coated on top of a 2.0wt .% Y2O3-added carbon preform, and reaction bonded silicon carbide (RBSC) was prepared by infiltrating molten Si at 1,450oC for 1-8 h. Reactive sintering of the Y2O3-free carbon preform caused Si to be pushed to one side, thereby forming cracking defects. However, when prepared from the Y2O3-added carbon preform, a SiC-Si composite in which Si is homogeneously distributed in the SiC matrix without cracking can be produced. Using the Si + C → SiC reaction at 1,450oC, 3C and 6H SiC phases, crystalline Si, and Y2O3 were generated based on XRD analysis, without the appearance of graphite. The RBSC prepared from the Y2O3-added carbon preform was densified by increasing the density and decreasing the porosity as the holding time increased at 1,450oC. Dense RBSC, which was reaction sintered at 1,450oC for 4 h from the 2.0wt.% Y2O3-added carbon preform, had an apparent porosity of 0.11% and a relative density of 96.8%.

목차
Abstract
1. 서 론
2. 실험방법
3. 결과 및 고찰
4. 결 론
References
저자
  • 장민호(금오공과대학교/(주)오렌지이앤씨) | Min-Ho Jang (Department of Advanced Materials Science & Engineering, Kumoh National Institute of Technology/Orange E& C)
  • 조경식(금오공과대학교) | Kyeong-Sik Cho (Department of Advanced Materials Science & Engineering, Kumoh National Institute of Technology) Corresponding Author