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재사용 열보호시스템용 경량 단열소재 및 코팅제조와 고온 성능평가 KCI 등재

Fabrication and High-Temperature Performance Evaluation of Light-Weight Insulation Materials and Coatings for Reusable Thermal Protection Systems

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Light-weight ceramic insulation materials and high-emissivity coatings were fabricated for reusable thermal protection systems (TPS). Alumina-silica fibers and boric acid were used to fabricate the insulation, which was heat treated at 1250 °C. High-emissivity coating of borosilicate glass modified with TaSi2, MoSi2, and SiB6 was applied via dip-and-spray coating methods and heat-treated at 1100°C. Testing in a high-velocity oxygen fuel environment at temperatures over 1100 °C for 120 seconds showed that the rigid structures withstood the flame robustly. The coating effectively infiltrated into the fibers, confirmed by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction analyses. Although some oxidation of TaSi2 occurred, thereby increasing the Ta2O5 and SiO2 phases, no significant phase changes or performance degradation were observed. These results demonstrate the potential of these materials for reusable TPS applications in extreme thermal environments.

목차
1. Introduction 
2. Experimental procedure 
3. Results and discussion 
    3-1. 경량 고온 세라믹 단열소재의 제조 및 공정개선 
    3-2. 고방사율 코팅소재의 제조 
    3-3. 고온내구성 평가 
4. Conclusion 
Funding
Conflict of Interest  
Data Availability Statement 
Author Information and Contribution 
Acknowledgement
References
저자
  • 남민수(한국세라믹기술원 이천분원 엔지니어링소재센터, 고려대학교 신소재공학과) | Min-Soo Nam (Engineering Materials Center, Korea Institute of Ceramic Engineering and Technology, Icheon, Gyeonggi-do, 17303, Republic of Korea, Department of Materials Science and Engineering, Korea University, Anam-dong, Seongbuk-gu, Seoul, 02841, Republic of Korea)
  • 김종일(한국세라믹기술원 이천분원 엔지니어링소재센터) | Jong-Il Kim (Engineering Materials Center, Korea Institute of Ceramic Engineering and Technology, Icheon, Gyeonggi-do, 17303, Republic of Korea)
  • 김성원(한국세라믹기술원 이천분원 엔지니어링소재센터) | Seongwon Kim (Engineering Materials Center, Korea Institute of Ceramic Engineering and Technology, Icheon, Gyeonggi-do, 17303, Republic of Korea) Corresponding author
  • 신재성(한국항공우주연구원 소형발사체연구부) | Jaesung Shin (Small Launch Vehicle Research Division, Korea Aerospace Research Institute, 169-84 Gwahak-ro, Yuseong-Gu, Daejeon, 34133, Republic of Korea)
  • 김현준(한국항공우주연구원 소형발사체연구부) | Hyeonjun Kim (Small Launch Vehicle Research Division, Korea Aerospace Research Institute, 169-84 Gwahak-ro, Yuseong-Gu, Daejeon, 34133, Republic of Korea)
  • 오범석(한국항공우주연구원 발사체기술연구1부) | Bum-Seok Oh (Launch Vehicle Technology Research Division (1), Korea Aerospace Research Institute, 169-84 Gwahak-ro, Yuseong-Gu, Daejeon, 34133, Republic of Korea)