This study investigated the correlation between compound malodor and total hydrocarbons (THC) to evaluate the potential use of THC as a predictor of compound malodor. A total of 87 samples were analyzed from five target facilities: two petrochemical manufacturing facilities (A, B), a wastewater treatment facility (C), a recycled plastic injection molding facility (D), and a surfactant manufacturing facility (E). The correlation coefficients of compound malodor and THC for each facility were as follows: A: 0.6698, B: 0.8068, C: –0.2767, D: 0.2071, and E: 0.7695. The correlation coefficient for all facilities was 0.5634, indicating a weak correlation. The coefficients of determination for the regression analysis to predict the compound malodor for facilities A, B, and E were 0.4093, 0.6316, and 0.5695, respectively, which validated the results of the correlation analysis. These values improved to 0.8394, 0.6941, and 0.7476 in the multiple regression analysis with the VOC analysis results added as independent variables. Therefore, it is expected that THC measurement that considers the characteristics of the facility can be used to establish a systematic odor management plan.