Solid phase microextraction (SPME) was used for the determination of 6 standard solvents (methanol, isopropanol, methyl ethyl ketone, ethyl acetate, cyclohexane, toluene) in food packaging materials. SPME method is a solvent-free sample preparation technique in which a fizsed silica fiber coated with polymeric organic liquid is introduced into the headspace above the sample. SPME method using fiber coated polydimethylsiloxane (PDMS) was compared with static headspace (SHS) method used as a reference. It was found that the optimal adsorption condition using PDMS-SPME method was 20 for 15 minutes for the standard solvents. Detection limits, linearity, reproducibility, and recovery of both SHS and PDMS-SPME methods have been determined using 6 standard solvents. Both methods were characterized by high reproducibility and good linearity. Using SHS method, the mean recovery of the 6 standard solvents was ranged from 75.5% to 105.8% with a mean relative standard deviation (RSD) of 0.3% to 4.8%. With PDMS-SPME method, the mean recovery of the 6 standard solvents was ranged from 86.7% to 108.3% with a mean RSD of 0.4% to 2.5%. The detection limits of both methods were the same for toluene, cyclohexane and methyl ethyl ketone; those of PDMS-SPME method were higher than those of SHS method for methanol, isopropanol and ethyl acetate. PDMS-SPME fiber showed excellent adsorption for non-polar solvents such as toluene, while it showed relatively low adsorption for polar solvents such as methanol.

This study was examined the current situation of utilization of meat broth materials for the development of various broth products. The 500 housewives living in Seoul were asked. The results obtained as follows; Beef(93%) was used most frequently for making broth. In order to reduce rancid smell of broth, garlic(72%), ginger(68%), green onion(60%), onion(58%), black pepper(44%), radish(25%) were used. Most housewives used beef three or four times a month and hardly used chicken or pork for making broth. Commercial broth materials were used two or three times a month. For making broth the bricket of beef, a whole or half chicken and bones of pig were consumed most frequently. Before making broth, from flesh only blood was removed. Also housewives slightly boiled bone blood-removed in water. The older age is, the longer marriage duration is, the higher monthly income and education level is, the more beef was consumed. The higher the education level is, the more vegetables like garlic, ginger, green onion, onion, radish were used. It is suggested that in order to develop various broth products made of natural materials, the characteristics of preferred broth materials should be defined and it is necesarry to accomplish the preference test of preferred broth products.

삼차원적 골격구조를 가지며 세공의 크기와 산성도가 유사한 SAPO-44, SAPO-34(CHA type), SAPO-17(ERI type), 그리고 1차원적 고격구조를 가진 ZSM-23(MTT type) 촉매재료를 합성하고, 메탄올 전환방응에 있어서의 촉매적 성능을 비교 검토하였다. 이들의 산성도 세기는 SAPO-44>SAPO-34>SAPO-17>ZSM-23 순으로 나타났다. 메탄올 전환반응을 비교한 결과, 삼차원적 골격구조를 가지고 있는 SAPO-34와 SAPO-44에서 높은 에티렌 선택성이 얻어졌으며, 특히 Ni을 골격내에 도입시켰을 때 그 선택율은 더욱 증가하였다. 반면에 1차원적 골격구조를 가지고 있는 ZSM-23에서는 입체적 형상선택성의 감소로 올레핀보다는 파라핀의 선택율이 우세하였다.

Hard materials such as hardmetal, coated hardmetal, cermet, ceramics and diamond or c-BN sintered compact are a kind of grain-dispersed alloy with high volume of hard particles. These are used for cutting tools, wear-resistant tools, rock bits, high pressure apparatus, etc. The annual production in Japan is about 1.7 billion dollars (200 billion yen). This is greatly owed to the development in science and technology which has been accomplished by applying new concepts such as fine or uniform grain microstructure, orientation of crystal grains, functionally graded material, artificial lattice and coherent bonding in recent years. In this review, the development in recent years in Japan is briefly summarized.

결량화 되고 고강도의재료를 요하는 자동차, 항공기, 선박, 각종 구조물 등 여러 분야에서 복합재료의 사용은 증가되어 왔고, 그에 따라 연구가 활발히 진행되고 있다. 본 연구에서는 Impulse Excitation Method을 통해 Transversely Isotropic한 재료의 공진 주파수를 측정함으로써 복합재료의 탄성계수를 구하였다. Timoshenko Beam Equation식에 나타나는 회전관성효과와 전단변형을 고려하였을 때와 고려하지 않았을 때 재료의 탄성계수에 변화가 어떻게 나타나는 가를 관찰하였다.

Research activities of Russian Medical Engineering Center and Institute of Medical Materials of Shape Memory Alloys and Implants are presented as follows: The direction of elaboration of porous shape memory alloys for medicine. Medical and technical requirements and physical and mechanical criteria of porous shape memory implants elaboration. Basic laws of heat-, stress- and strain-induced changes of mechanical properties, shape memory effect and superelasticity in porous TiNi-based alloys. Methods of regulation of shape memory effect parameters in porous alloys and methods for controlling the regulation-induced changes of physical and mechanical properties. Original technologies of elaboration of porous alloys In various fields of medicine. Arrangement of serial production of shape memory porous implants and examples of their medical use.

방사선물질의 수송 및 저장용기 등에 사용되는 에폭시수지계 중섣자 차폐재, KNS-201, KNS-301 및 KNS-601을 제조하였다. 기본물질은 개질 및 수소 첨가된 비스페놀 A형 그리고 노블락형 에폭시수지이며, 첨가제로는 수산화알루미늄 및 탄화붕소이다. 이들 중성자 차폐재들의 열적 및 역학적 성질 및 재방사선성 등을 평가하기 위해 여러 특성시험을 행하였다. 조사된 제반 특성들은 열분해온도;257~280˚C, 열전도도;0.95~1.14W/m.K, 열팽창계수 ;0.77~1.26x10-6˚C-1, 연소특성;800˚C이하, 평균연소시간;5초 이하, 평균연소길이 ;5mm 이하, 인장강도;2.5~3.2Kg/mm2,압축강도:13.2~15.2kg/mm2 굴곡강도:5.2~604Kg/mm2 등을 나타냈다. 전반적으로 개발된 중성자 차폐재들의 관련 특성들이 외국에서 사용되는 중성자 차폐재, NS-4-RF보다 우수한 것으로 나타났다. 또한 KNS-601의 내방사선성이 KNS-201과 KNS-301보다 우수한 것으로 나타났다. 또한 KNS-601의 내방사선이 KNS-201과 KNS-301보다 우수한 것으로 나타났다.

The purpose of this study is to connect the technics and form from ancient to Korea Dynast But in these period there is no buildings remains but paintings, fine arts, and stupas. In the historical materials there are many architectural form and signature revealings, so as a result these analysis, 1)The building showed in paintings of Silla, and Korea Dynasty reflect the architectural style their own Dynasty. 2)In detail, the architecture of Silla and Korea Dynasy was connected with Chinese architectur Liao, Song. But from the 8Century Koreans were succeeded the one of Silla Dynasty and had originility in architectural style. 3)The architectursl style in Silla and Korea Dynasty were very various and very rich content. And we must more serious study of historical materials so that we improve the ancient a middle age of architcture in Korea.