Metakaolin-based geopolymers have shown promise as suitable candidates for 14C immobilization and final disposal. It has been shown that the physicochemical properties of metakaolin wasteforms meet, and often far exceeding, the strict compression strength and leaching acceptance criteria of the South Korea radioactive waste disposal site. However, it is not possible to analyze and characterize the internal structure of the geopolymer wasteform by conventional characterization techniques such as microscopy without destruction of the wasteform; an impractical solution for inspecting wasteforms destined for final disposal. Internal inspection is important for ensuring wastes are homogenously mixed throughout the wasteform and that the wasteform itself does not pose any significant defects that may have formed either during formulation and curing or as a result of testing prior to final disposal. X-ray Computed Tomography (XCT) enables Non-Destructive Evaluation (NDE) of objects, such as final wasteforms, allowing for both their internal and external, characterization without destruction. However, for accurate quantification of an objects dimensions the spatial resolution (length and volume measures) must be know to a high degree of precision and accuracy. This often requires extensive knowledge of the equipment being used, its precise set-up, maintenance and calibration, as well as expert operation to yield the best results. A spatial resolution target consists of manufactured defects of uniformed dimensions and geometries which can be measured to a high degree of accuracy. Implementing the use of a spatial resolution target, the dimensions of which are known and certified independently, would allow for rapid dimensional calibration of XCT systems for the purpose of object metrology. However, for a spatial resolution target to be practical it should be made of the same material as the intended specimen, or at least exhibit comparable X-ray attenuation. In this study, attempts have been made to manufacture spatial resolution targets using geopolymer, silica glass, and alumina rods, as well as 3D printed materials with varying degrees of success. The metakaolin was activated by an alkaline activator KOH to from a geopolymer paste that was moulded into a cylinder (Diameter approx. 25 mm). The solidified geopolymer cylinder as well as both the silica glass rod and alumina rod (Diameter approx. 25 mm) we cut to approximately 4 mm ± 0.5 mm height with additional end caps cut measuring 17.5 mm ± 2.5 mm height. All parts were then polished to a high finish and visually inspected for their suitability as spatial resolution targets.