YAG phosphor powders were fabricated by the atmospheric plasma spraying method with the spray-dried spherical YAG precursor. The YAG precursor slurry for the spray drying process was prepared by the PVA solution chemical processing utilizing a domestic easy-sintered aluminum oxide (Al2O3) powder as a seed. The homogenous and viscous slurry resulted in dense granules, not hollow or porous particles. The synthesized phosphor powders demonstrated a stable YAG phase, and excellent fluorescence properties of approximately 115% compared with commercial YAG:Ce3+ powder. The microstructure of the phosphor powder had a perfect spherical shape and an average particle s ize of a pprox imately 30 μm. As a r esult of t he PKG t est of t he YAG p hosphor p owder, t he s ynthesized phosphor powders exhibited an outstanding luminous intensity, and a peak wavelength was observed at 531 nm.
To improve the safety of nuclear fuel, research on the advanced nuclear fuel (UO2) by adding various trace elements is being conducted. For example, the addition of metals such as Mo, Cr can improve the thermal conductivity of nuclear fuel, minimizing the diffusion of fission products. Trace metal oxide additives (SiO2, Cr2O3, Al2O3, etc.) can suppress the release of fission gases. In general, complete dissolution of the fuel sample is required for chemical analysis to determine its elemental compositions. Among widely used metal oxide additives, aluminum oxide is difficult to dissolve in nitric acid due to its excellent thermal and chemical stability. In this study, we investigated on different chemical dissolution methods by applying a microwave digestion system under various acid solutions. We confirmed the validity of the digestion method by carrying out trace element analysis using an Inductively-Coupled Plasma Atomic Emission Spectrometer (ICP-AES).