Sweet persimmons are valuable commodity in the export market. However, present of insect pest such as Asiacornococcus kaki can cause limit to many export markets. In this study, ethyl formate(EF), as alternative to methyl bromide(MB), was used in scale-up commercial trial(20ft reefer). Application of 50 g/m3 of EF for 6 hours at 5 ℃ showed proven efficacy against all developmental stages of A. kaki without LLDPE-packaging fruits and no phytotoxic damage on sweet persimmons. This study demonstrated that EF fumigation can be effectively control to target A. kaki before packaging with LLDPE-film of fruits.