When self-disposing of radioactive waste, it is important to follow the acceptable concentration standards for each nuclide set by the Nuclear Safety and Security Commission (NSSC). Gamma-emitting nuclides can be easily analyzed with a simple pretreatment process, but beta-emitting nuclides require a chemical separation procedure to be analyzed for radiochemistry analysis. When analyzing betaemitting nuclides for the purpose of self-disposal, there may be difficulties in radiation detection after the chemical separation process. This is because the concentration of beta nuclides in the sample may be low and some of them may be lost during the chemical separation. Therefore, measurement method of gross-beta activity can be used instead of that of each nuclide to access the compliance of selfdisposal criteria. While a proportional counter is commonly used to measure gross-beta activity, liquid scintillation counting can also be used to measure gross-beta, and we plan to compare the results of both methods.