The purpose of this study was to process extraction and separation for polyglucose porpyran from pophyra yezoensis as high yield. The acidic porphyran solution was extracted with 0.1∼1N of α,β-dichloromaleic acid or α-chloromaleic acid of 2% solution as organic acid instead of inorganic acid at 60℃ and then porphyran was collection of high yield to acidic solution and it was neutralization treated with 0.1N of d-Ca(OH)2 solution and the mixture was conversion to porphyran salt form and treated with a shell powder of ouster and then added of ethanol as precipitator. It recovery porphyran contained of violet purple laver coloring matter was obtained as a crystalline and used for the next step without future purification to prepare of porphyran laver jam. so, The resulting porphyran and porphyran jam was characterized by it component and physical properties.