The current concern about these materials (MoSi2 and NbSi2) focuses on their low fracture toughness below theductile-brittle transition temperature. To improve the mechanical properties of these materials, the fabrication of nanostructuredand composite materials has been found to be effective. Nanomaterials frequently possess high strength, high hardness, excellentductility and toughness, and more attention is being paid to their potential application. In this study, nanopowders of Mo, Nb,and Si were fabricated by high-energy ball milling. A dense nanostructured MoSi2-NbSi2 composite was simultaneouslysynthesized and sintered within two minutes by high-frequency induction heating method using mechanically activated powdersof Mo, Nb, and Si. The high-density MoSi2-NbSi2 composite was produced under simultaneous application of 80MPa pressureand an induced current. The sintering behavior, mechanical properties, and microstructure of the composite were investigated.The average hardness and fracture toughness values obtained were 1180kg/mm2 and 3MPa·m1/2, respectively. These fracturetoughness and hardness values of the nanostructured MoSi2-NbSi2 composite are higher than those of monolithic MoSi2 orNbSi2.

Nanocrystalline materials have received much attention as advanced engineering materials with improved physical and mechanical properties, including high strength, high hardness, excellent ductility and toughness. In this study, nanopowders of Al2O3, MgO and TiO2 were prepared as starting materials by high energy ball milling for the simultaneous synthesis and sintering of the nanostructured compound Mg4Al2Ti9O25 by high-frequency induction heating process. The highly dense nanostructured Mg4Al2Ti9O25 compound was produced within one minute by the simultaneous application of 80MPa pressure and induced current. The sintering behavior, grain size and mechanical properties of the Mg4Al2Ti9O25 compound were evaluated.

This study deals with the high frequency induction hardening (HF at 850℃, 120kHz & 50kW condition) SM45C steel. (1) The HF specimen, which was tempered at 150℃, did not show any tempering effect. A brittle fracture occurred at rounded area of the tensile specimen. AE (acoustic emission) amplitude distribution showed between 45dB and 60dB. (2) A slip and fracture occurred at the hole area of the HF specimen which was tempered at 300℃. As they pass the yield point, the AE energy is increased intermittently and AE amplitude distribution exists between 70dB and 85dB. In addition, after imposing the maximum tensile load, AE signals showed high amplitude and energy distribution. The AE amplitude showed between 45dB and 70dB. (3) A brittle fracture occurred at HF specimen which was tempered at 450℃ as if it is torn in the direction of 45° on parallel area over the both sides of the tensile specimen, which lead to several peak appeared in AE energy. It was found that the AE amplitude was relatively low and the AE energy was high.

This study is deal with the high frequency induction hardening (HF at 850℃, 120kHz & 50kW condition) SM45C steel. (1) The HF specimen which was tempered at 150℃, did not appear any tempering effect. A brittle fracture occurred at rounded area of the tensile specimen. AE amplitude distribution showed between 45~60dB. (2) The HF specimen which was tempered at 300℃, slip and fracture occurred at the hole area of the tensile specimen. As it passes the yield point, the AE energy increased intermittently and AE amplitude distribution showed between 70~85dB. In addition, after the maximum tensile load, it showed high amplitude and energy distribution. The AE amplitude showed between 45~70dB. (3) The HF specimen which was tempered at 450℃, a brittle fracture occurred as if it is torn in the direction of 45℃ on parallel area over the both sides of the tensile specimen, which led to several peak to be appeared in AE energy. It was found that the AE amplitude was relatively low and the AE energy was high.

Nanopowders of and FeAl were fabricated by high energy ball milling. Dense 4.25 composite was simultaneously synthesized and consolidated by high frequency induction heated combustion method within 2 min from mechanically activated powders. Consolidation was accomplished under the combined effects of a induced current and mechanical pressure of 80 MPa.

Nanostructured was synthesized to have high density via rapid and cost effective process named as high-frequency induction heated combustion synthesis(HFIHCS) method. For the process, mechanically activated Re-Si powder was used, which had been prepared by mechanical ball milling of Re and Si powders with mixing ratio of 1:1.75. Both combustion synthesis and densification were accomplished simultaneously by applying electric current and mechanical pressure of 80 MPa during the process. The average grain size, hardness, and fracture toughness of the compound were 210 nm, 1085 and 4 , respectively. The experimental results show that HFIHCS is a promising process for synthesis of nanostructured which has a potential for both high temperature and thermo-electric applications

Dense nanostructured was synthesized by high-frequency induction-heated combustion synthesis (HFIHCS) method within 1 minute in one step from mechanically activated Nb and Si powders. Highly dense with relative density of up to 99% was simultaneously synthesized and consolidated under the combined effects of an induced current and mechanical pressure of 60 MPa. The average grain size and mechanical properties (hardness and fracture toughness) of the compound were investigated

In this study, hydroxyapatite (HAp) and hydroxyapatite-yttria stabilized zirconia (HAp-3YSZ) with 20 vol. %– (ZrO2+3 %mol Y2O3) nanopowders were consolidated very rapidly to full density by High-frequency induction heat sintering (HFIHS). Effects of temperature and the addition of 3YSZ on the toughness, hardness and microstructure properties have been studied. 3YSZ second phase toughening HAp composites with higher toughness were successfully developed at relatively low temperatures through this technique. Compared with hardness and toughness obtained for pure HAp, the hardness and toughness for HAp-20vol. % 3YSZ were much higher.

Nanostructured Alumina - 20 vol% 3YSZ composites powder were synthesized by wet-milling technique. The starting materials were a mixture of Alumina micro-powder and 3YSZ nano-powders. Nano-crystalline grains were obtained after 24 h milling time. The nano-structured powder compacts were then processed to full density at different temperatures by high-frequency induction heat sintering (HFIHS). Effects of temperature on the mechanical and microstructure properties have been studied. composites with higher mechanical properties and small grain size were successfully developed at relatively low temperatures through this technique.

고주파유도가열 연소합성법으로 60MPa의 기계적 압력과 고주파유도가열 장치의 총용량 (15KW)의 90%의 출력을 가해 75초의 짧은 시간에 97%이상의 상대밀도를 갖는 복합체를 제조하였으며, 제조된 시편의 미세조직 사진으로부터 선형분석법으로 측정한 의 평균 결정립크기는 각각 250nm 과 60nm 이었다. 또한 제조된 시편을 연마하여 비커스 경도계를 이용하여 기계적 특성평가를 한 결과 경도 와 파괴인성은 각각 와 이었다.

Dense -20vol.%SiC composite was synthesized by high-frequency induction-heated combustion synthesis(HFIHCS) method within 2 minutes in one step from elemental powder mixture of W, Si and C. Simultaneous combustion synthesis and densification were accomplished under the combined effects of an induced current and mechanical pressure. Highly dense -20vol.%SiC with relative density of up to 97% was produced under simultaneous application of 60MPa pressure and the induced current. The average grain size of was about 5.2. The hardness and fracture toughness values obtained were 1700kg/ and , respectively.

Using the high-frequency induction heated combustion method, the simultaneous synthesis and densification of (x=0, 10, 20, 30) composites was accomplished using elemental powders of W, Si and C. A complete synthesis and densification of the materials was achieved in one step within a duration of 2 min. The relative density of the composite was up to 97% for the applied pressure of 60MPa and the induced current. The average grain size of are 6.9, 6.1, and , respectively. The hardness and the fracture toughness increases with increasing SiC content. The maximum values for the hardness and fracture toughness are .

Using a developed high-frequency induction heated combustion method. the simultaneous synthesis and densification of WC-xvol.%Co() hard materials was accomplished using elemental powders of W, C and Co. A complete synthesis and densification of the materials was achieved in one step within a duration of 1min. The final relative densities of the composite were over 98.5% for all cases, under the applied pressure of 60 MPa and the induced current. The hardness of the composites decreases and the fracture toughness increases with increasing cobalt content. As the carbon to tungsten ration increases, the hardness increase, but the fracture toughness decreases. The maximum values for the fracture toughness and hardness are 15.1 (at 20vol.%Co, W:C=1:1), and 1928 (at 5vol.%Co, W:C=1:1.3), respectively. Therefore we concluded that the HFIHCS method. which can produce WC-xvol.%Co within 1 minute in one step is superior to conventional ones.

1) Using a developed high-frequency induction heated sintering method, the rapid densification of WC-Co hard materials was accomplished using ultra fine powders with 260 nm size within 1 minute. 2) The relative density of the composite was 99.5% for the applide pressure of 60MPa and the induced current for 90% output of total capacity. 3) The grain size of WC-Co hard materials is about 260nm and the average thickness of the binder phase determined is about 11nm. The fracture toughness and the hardness of this work 12 , respectively. 4) Using pressureless sintering, we produced dense WC-Co hard materials with a relative density of 97% without applying pressure.