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        검색결과 6

        1.
        2023.11 구독 인증기관·개인회원 무료
        In KAERI’s previous phosphate precipitation tests, the dispersed powder of lithium phosphate (Li3PO4) as a precipitation agent reacted with various metal chlorides in a simulated LiCl-KCl molten salt. The reaction of metal chlorides composed of actinides such as uranium and three rare earths (Nd, Ce and La) with lithium phosphate is a solid-liquid reaction. A phosphorylation reaction rate is very fast and the metal phosphates as a reaction product precipitated on the bottom of the molten salt crucible. One of the recovery methods of the metal phosphate precipitates is segregation the lower part (precipitates) of the salt ingot using the various cutting tools. Recently, a new phosphorylation experiment using lithium phosphate ingots carried out in order to collect the metal phosphate precipitates into a small recovering vessel, and the test result of this new method was feasible. However, the reaction rate of test using lithium phosphate ingot is extremely slower than that of test using lithium phosphate powder. In this study, the precipitation reactor design (a tapered crucible with polished inner surface) used for phosphorylation reaction showed that the salt ingot with metal phosphate precipitates could be detached from a tapered stainless steel crucible. We propose that the recovery of precipitates from a salt ingot is possible by introducing a dividing plate structure into a molten salt and by positioning it at the interface between salt and precipitated metal phosphate.
        4.
        2018.04 KCI 등재 구독 인증기관 무료, 개인회원 유료
        Spherical monosized pure aluminum (Al) particles are successfully fabricated by the pulsated orifice ejection method (POEM). The surface reaction between Al and the graphite crucible is investigated by analysing the microstructure and chemical composition of the materials. No significant chemical reaction occurs between Al and the graphite owing to the crystalline Al oxide (γ-Al2O3) layer generated in the initial state. The γ-Al2O3 layer is clearly observed in all regions between the Al particles and graphite via transmission electron microscopy and confirmed by the selected area diffraction pattern. The morphology of the γ-Al2O3 layer perfectly follows the surface morphology of the graphite crucible, which showed nanoscale roughness. This implies that molten Al could not directly contact graphite even though the surface of the crucible became rough to some extent. However, this passivation phenomenon allowed the successful fabrication of monosized pure Al particles. Therefore, POEM is a useful process at least to manufacture monosized pure Al particles.
        4,000원
        6.
        2016.12 KCI 등재 구독 인증기관 무료, 개인회원 유료
        This study aims to re-read aspects of violence reproduced in The Crucible through the theories of violence of Walter Benjamin, Slavoj Žižek and Hannah Arendt. This study intends to re-read The Crucible through the theories of violence of Benjamin, Žižek and Arendt because of what they commonly emphasized, that is, the fact that escape from stereotype image of violence provides significant implications for contemplation on violence. When we re-read The Crucible by taking one step back from the power of accusation wrapped in fury and lunacy and taking notice on stark law-making and law-preserving nature of Salem society, foundation can be created to contemplate and reflect on its ‘systemic violence.’ In addition, Arendt’s theory of violence which saw opposing relationship between ‘violence’ and ‘power’ and between ‘behavior’ and ‘action’ provides insight into the origin of witch hunt in Salem society and into understanding the meaning of John Proctor’s resistance.
        5,500원