In 1997, Dr. James Chien-Min Sung patented the technology of making diamond tools according to a predetermined pattern. The optimization of this pattern may double the tool life and the cutting speed. In 1998, Sung also made DiaGrid® saw segments that showed superior performance in cutting granite and marble. In 2000, Sung visited Shinhan and introduced them this revolutionary concept of diamond saw segments. In 2005, Shinhan adapted the idea and produced saw segments with diamond grits set in a predetermined pattern, their results confirmed that the sawing speed and the sawing life were both improved over conventional designs.

For dry machining of mineral materials the Institute of Materials Engineering pursues a novel thermal protection shield concept for diamond tools, in which thermal insulating materials in diamond composite structures act as heat shield, which protects diamonds in deeper layers against high temperature and graphitisation. Before the effectiveness of this concept could be investigated suitable composites have to be manufactured. In this paper the powder metallurgical production processes of diamond-alumina-cobalt-composites with varying alumina and cobalt particle sizes, their microstructures and porosities are described. It could be observed that the distribution of small-sized alumina particles (<70μm) in the cobalt matrix is uniform and the porosity of the composite decrease.

Nowadays the market for diamond tools grows rapidly. The present decline in the price of industrial diamond makes it a commoditised product capable of competing with conventional abrasives. In terms of production volume, the largest group of diamond tools comprises the metal-bonded diamond impregnated tools, such as sawblades, wire saws, and core drills for cutting stone and construction materials, and core bits for mining applications. This article provides a compendious coverage of the powder metallurgy (PM) diamond tool-making routes, and identifies the recent trends towards changing the tool design and composition to render it cheaper and more efficient.

현재 도로분야에서 콘크리트 포장의 양적증가와 공용연수 증가로 콘크리트 포장의 손상에 따른 유지보수문제가 크게 부각되기 시작했다. 국내에서 적용되고 있는 콘크리트 포장 유지보수는 통상 손상된 부위의 부분보수후 아스팔트 덧씌우기 공법을 일괄적으로 적용하고 있다. 본 연구에서는 콘크리트 포장의 예방적 유지관리공법인 다이아몬드 그라인딩 공법에 대한 적용기준 평탄성, 미끄럼저항성, 소음, 경제성, 포장의 수명연장등 이론적인 연구를 수행하고, 이를 바탕으로 시험시공을 실시하여 초기공용성에 대한 측정을 실시하였다. 종단평탄성측정은 ARAN의 차륜부 좌우에 별도의 평탄성 측정센서를 부착 자동측정차량을 통해 시공전 후의 평탄성을 측정하였다. 미끄럼저항성은 SN기준값으로 분류하여 다이아몬드 그라인딩 시공전 후의 차로별 미끄럼 저항값을 측정하였다. 소음측정은 시공구간과 일반구간, 차종, 속도를 변수로 선정하여 소음발생정도를 측정하였고, 시공전 후의 평균조도깊이를 측정하여 다이아몬드 그라인딩 공법의 평가를 실시하였다. 분석결과 종단평탄성은 시공후 6%~40%가 향상되었으며, 미끄럼저항성은 1차로에서 66%, 2차로에서 37%의 증진효과가 있었다. 소음은 다이아몬드 그라인딩 구간에서 평균 3.4dB의 소음감소 효과가 나타났으며, 평균조도 깊이는 79%의 깊이 항상 효과를 보였다. 그러므로, 향후 기존 콘크리트 포장의 유지보수공법으로서 다이아몬드 그라인딩 공법의 국내적용이 적정하다고 판단된다.

This paper described the preparation method for composing high-grade synthetic diamond by water atomizing using FeNi30 powder catalyst. The objective of this article is about powder making process using super high water atomizing in the atmosphere of inert gas, and then corroded the powder with a corrosion inhibitor. Finally, FeNi30 catalyst powder with lower oxygen content and good sphericity is produced. The experiment of making diamonds by using cubic press and the performance of the diamonds are also discussed.

Metal/diamond binary composite coatings on Al substrate without grit blasting were deposited by cold spray process with insitu powder preheating. Microstructural characterization of the as-sprayed coatings with different diamond size, strength and with/without Ti coating on diamond was carried out by OM and SEM. The assessment of basic properties such as tensile bond strength and hardness of the coatings, and the deposition efficiency was also carried out. Particular attention on the composite coatings was on the diamond fracture phenomenon during the cold spray deposition and the interface bonding between the diamond and the Fe-based metal matrix.

The purpose of the present study is to determine an optimum composition using cheaper powders keeping with high performance of hard rock cutting diamond saw blade. With 50Fe-20(Cu . Sn)-30Co specimen, a part of Co was replaced by Ni(5%, 10%, and 15%, respectively). These specimens were hot pressed and sintered for predetermined time at various temperature. Sintering is performed by two different methods of temperature controlled method and specimen dimension controlled method. In order to determine the property of the sintered diamond saw blade, 3 point bending tester, X-ray diffractometer, and SEM were used. As the Co in the bond alloy was replaced by Ni, the hardness of the specimen increased. Thus the 50Fe-20(CuㆍSn)-15Co-15Ni specimen showed the maximum hardness of 104(HRB). The results of 3 point bending test showed that flexure strength decreased along with increase in Ni content. This is attributed to the formation of intermetallic compound(NiSn) determined by X-ray diffraction. The fracture surface after 3 point bending test showed that diamond was fractured in the specimen containing 0%, 5%, and 10%Ni, and the fracture occurred at the interface between diamond and matrix in the specimen containing 15%Ni. The cutting ability test showed that the abrasive property was not changed in the specimen containing 0%, 5%, and 10%Ni. The optimum composition determined in this study is 50Fe-20(CuㆍSn)-20Co-10Ni.

Ni-diamond composite powders with nickel layer of round-top type on the surface of synthetic diamond (140/170 mesh) were prepared by the electroless plating method (EN) with semi-batch reactor. The effects of nickel concentration, feeding rates of reductant, temperature, reaction time and stirring speeds on the weight percentage and morphology of deposited Ni, mean particle size and specific surface area of the composite powders were investigated by Atomic Adsortion Spectrometer, SEM-EDX, PSA and BET. It was found that nucleated Ni-P islands, acted as catalytic sites for further deposition and grown into these relatively thick layers with nodule-type on the surface of diamond by a lateral growth mechanism. The weight percentage of Ni in the composite powder increased with reaction time, feeding rate of reductant and temperature, but decreased with stirring speed. The weight percentage of Ni in Ni-diamond composite powder was 55% at 150 min., 200 rpm and 7 .

The inter-particle distance between diamonds on the segment surface of sawing blade predicted theoretically and measured experimentally followed a Gamma or Weibull function, rather than a normal distribution function. These results suggest that random dispersion of diamond particles in the segment may not be an efficient way of improving cutting efficiency of the blade.

Distributions of diamond particles protruding on the surface of worn diamond segments in circular saw has been investigated. Scanning electron microscope was used to examine the worn ,surface and radial saw blade wear and grinding ratio was measured. The number of protruded diamond particle was approximately 50% of the total number of particles, and that was independent of diamond particle concentration and table speed. It was also noted that the inter-particle distance did not follow a symmetric function like Gaussian distribution function, instead it fitted well with a probability density function based on gamma function. The distribution of inter-particle spacing, therefore, was analyzed using a gamma function model.

rf PECVB법을 이용하여 붕규산 유리 기판 위에 diamond like carbon(DLC) 박막을 증착하였다. 메탄(CH4)-수소(H2) 혼합 가스를 전구체 가스로 사용하였다. DLC 박막의 형상, 구조 및 광학적 특성은 SEM, 라만 및 UV 스펙트럼으로 분석하였다. 증착 속도는 혼합 가스의 수소 농도에 따라 증가하다가, 혼합 가스 유량이 25 sccm 이상에서는 일정하게 되었다. UV스펙트럼으로 계산한 박막의 optical band gap은 증착 시간과 DC serf bias의 증가에 따라 감소하는 경향을 나타냈으나, 수소함량에 의해서는 거의 영향이 없었다. 박막의 투과율에 가장 큰 영향을 미치는 인자는, 특히 자외선 영역과 가시광선 영역에서, bias 전압이었다.

본 연구에서는 도핑하지 않은 다이아몬드 박막에서의 전류전도 경로를 체계적으로 규명하고 다이아몬드 박막의 전도기구에 대해 조사하였다. 도핑되지 않은 다결정 다이아몬드 박막에서 두께와 측정방향에 따른 교류 임피던스법에 의해 측정된 저향값이 기존의 표면전도 모델과는 일치하지 안니하였다. 다이아몬드 박막에 구리를 전기도금한 결과 구리는 결정립계에만 불연속적으로 도금되었고 다이아몬드 박막 위에 은을 증착한 후 전지에칭을 한 결과 결정립계가 우선 에칭이 되어 전류가 결정립계를 통하여 흐름을 확인하였다. 또, 리본형 다이아몬드 박막의 표면을 절연층으로 형성시킨 후 박막 내부의 결정립계를 통하여 전류가 흘러 전기도금이 되는 것으로부터 다결정 다이아몬드 박막의 주요 전기전도 경로는 결정립계임을 확인하였다. 높은 전기전도도를 보여주는 다이아몬드 박막은 전도 활성화 에너지가 45meV 정도이었고 dangling bond 밀도는 낮았다. 그러나 산소 열처리나 수소플라즈마처리가 Si passivation 이론과는 반대로 dangling bond 밀도를 증가시키면서 전기전도성을 떨어뜨렸다. 이 결과들과 표면의 탄소화학결합을 연결시켜 높은 전도성을 야기시키는 결합은 H-C-C-H 결합임을 추론하였다.