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마그네슘환원에 의한 C/N 조성제어 초미립 TiCxNy 분말 합성 KCI 등재

Preparation of Ultrafine C/N Controled TiCxNy Powders by Magnesium Reduction

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

The ultrafine titanium carbonitride () particles below 100 nm in mean size, including various carbon and nitrogen contents (x=0.55~0.9, y=0.1~0.5), were successfully synthesized by new Mg-thermal reduction process. Nanostructured sub-stoichiometric titanium carbide () particles were initially produced by the magnesium reduction of gaseous at and post heat treatments in vacuum were performed for 2 hrs to remove residual magnesium and magnesium chloride mixed with . Finally, well C/N-controled phases were successfully produced by nitrification heat treatment under normal gas atmosphere at for 2 hrs. The values of purity, mean particle size and oxygen content of produced particles were about 99.3%, 100 nm and 0.2 wt.%, respectively.

저자
  • 이동원 | Lee Dong-Won
  • 김병기 | Kim Byoung-Kee
  • 윤중열 | Yun Jung-Yeul
  • 유지훈 | Yu Ji-Hoon
  • 김용진 | Kim Yong-Jin