This study was performed to evaluate the contact toxicity and residual toxicity of the 26 commercially registered insecticides against cigarette beetle, Lasioderma serricorne and maize weevil, Sitophilus zeamais adult. Among 26 insecticides, seven insecticides (chlorpyrifos, chlorpyrifos-methyl, fenitrothion, fenthion, phenthoate, cypermethrin, α-cyhalothrin) against L. serricorne adult and five insecticides (chlorpyrifos, chlorpyrifos-methyl, fenitrothion, fenthion, phenthoate) against S. zeamais adult showed perfect mortality. LC50 (ppm) values of those selected insecticides were appeared lowest value on α-cyhalothrin (1.46 ppm) against L. serricorne adult and chlorpyrifos-methyl (0.64 ppm) against S. zeamais adult, respectively. However, chlorpyrifos-methyl still remain high toxicity until 90th days after treatment against both L. serricorne and S. zeamais adults. From above results, it will be useful information to select insecticides effective against L. serricorne and S. zeamais adults.