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하이드라진을 이용한 용액환원법에 의한 Ni-GDC 미분말 합성과 전기적 특성 KCI 등재 SCOPUS

Preparation of Ni-GDC Powders by the Solution Reduction Method Using Hydrazine and Its Electrical Properties

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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

Ni-GDC (gadolinia-doped ceria) composite powders, the anode material for the application of solid oxide fuel cells, were prepared by a solution reduction method using hydrazine. The distribution of Ni particles in the composite powders was homogeneous. The Ni-GDC powders were sintered at 1400˚C for 2 h and then reduced at 800˚C for 24 h in 3% H2. The percolation limit of Ni of the sintered composite was 20 vol%, which was significantly lower than these values in the literature (30-35 vol%). The marked decrease of percolation limit is attributed to the small size of the Ni particles and the high degree of dispersion. The hydrazine method suggests a facile chemical route to prepare well-dispersed Ni-GDC composite powders.

저자
  • 김선중 | Kim, Sun-Jung
  • 김강민 | 김강민
  • 조평석 | 조평석
  • 조윤호 | 조윤호
  • 이충용 | 이충용
  • 박승영 | 박승영
  • 강윤찬 | 강윤찬
  • 이종흔 | 이종흔