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수열합성법을 이용한 NiCrAl 합금 폼 위에 합성된 NiO 촉매 형상 제어 KCI 등재 SCOPUS

Morphology Control of NiO Catalysts on NiCrAl Alloy Foam Using a Hydrothermal Method

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  • URLhttps://db.koreascholar.com/Article/Detail/315866
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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

Flower-like nickel oxide (NiO) catalysts were coated on NiCrAl alloy foam using a hydrothermal method. The structural, morphological, and chemical bonding properties of the NiO catalysts coated on the NiCrAl alloy foam were investigated by field-emission scanning electron microscopy, scanning electron microscopy-energy dispersive spectroscopy, Xray diffraction, and X-ray photoelectron spectroscopy, respectively. To obtain flower-like morphology of NiO catalysts on the NiCrAl alloy foam, we prepared three different levels of pH of the hydrothermal solution: pH-7.0, pH-10.0, and pH-11.5. The NiO morphology of the pH-7.0 and pH-10.0 samples exhibited a large size plate owing to the slow reaction of the hydroxide (OH−) and nickel ions (Ni+) in lower pH than pH-11.5. Flower-like NiO catalysts (~4.7 μm-6.6 μm) were formed owing to the fast reaction of OH− and Ni2+ by increased OH− concentration at high pH. Thus, the flower-like morphology of NiO catalysts on NiCrAl alloy foam depends strongly on the pH of the hydrothermal solution.

목차
1. 서 론
 2. 실험 방법
 3. 결과 및 고찰
 4. 결 론
 Acknowledgements
 References
저자
  • 신동요(서울과학기술대학교 신소재공학과) | Dong-Yo Sin
  • 이은환(서울과학기술대학교 신소재공학과) | Eun-Hwan Lee
  • 박만호((주) Alantum) | Man-Ho Park
  • 안효진(서울과학기술대학교 신소재공학과) | Hyo-Jin Ahn Corresponding author