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HPLC를 이용한 사료 중 Deoxynivalenol, Zearalenone의 분석과 오염도 조사 KCI 등재

Analysis and Survey for Contamination of Deoxynivalenol and Zearalenone in Feed by High Performance Liquid Chromatography

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한국식품위생안전성학회지 (Journal of Food Hygiene and Safety)
한국식품위생안전성학회 (Korean Society of Food Hygiene and Safety)
초록

Deoxynivalenol (DON) and zearalenone (ZEN) are mainly contaminated mycotoxins in feeds. The study was carried out to analyze and survey the contamination of DON and ZEN in one hundred thirteen samples of feeds. After cleaning all samples with immunoaffinity column, the mycotoxins were analysed by using high performance liquid chromatography/fluorescence with diode array detector (HPLC /FLD with DAD). The average recoveries of DON were 88.76 and 95.40% at the levels of 200 and 1,000 μg/kg and 87.09 and 98.40% of ZEN were recovered at the levels of 100 and 500 μg/kg, respectively. The limit of detection (LOD) were 6.0 and 3.0 μg/kg for DON and ZEN, respectively. The average concentrations of DON were 372.1, 324.0 and 990.9 μg/kg in chicken, pig and cattle feed, respectively. Those of ZEN were 76.1, 43.7 and 196.2 μg/kg for them, individually.

저자
  • 김동호(국립농산물품질관리원)
  • 최규일(국립농산물품질관리원 시험연구소) | Choi Gyu Il
  • 홍경숙(국립농산물품질관리원)
  • 김현정(국립농산물품질관리원)
  • 송영진(국립농산물품질관리원)
  • 강승훈(국립농산물품질관리원)
  • 장한섭(국립농산물품질관리원)
  • 조현정(국립농산물품질관리원)
  • 한계수(국립농산물품질관리원)