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Preparation and Structure Properties of LaBa2Cu2O9, LaBa2CaCu3O12 and LaBa2Ca2Cu5O15 Perovskites KCI 등재 SCOPUS

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한국재료학회지 (Korean Journal of Materials Research)
한국재료학회 (Materials Research Society Of Korea)
초록

In this study we examine variations in the structure of perovskite compounds of LaBa2Cu2O9, LaBa2CaCu3O12 and LaBa2Ca2Cu5O15 synthesized using the solid state reaction method. The samples’ compositions were assessed using X-ray fluorescence (XRF) analysis. The La: Ba: Ca: Cu ratios for samples LaBa2Cu2O9, LaBa2CaCu3O12 and LaBa2Ca2Cu5O15 were found by XRF analysis to be around 1:2:0:2, 1:2:1:3, and 1:2:2:5, respectively. The samples’ well-known structures were then analyzed using X-ray diffraction. The three samples largely consist of phases 1202, 1213, and 1225, with a trace quantity of an unknown secondary phase, based on the intensities and locations of the diffraction peaks. According to the measured parameters a, b, and c, every sample has a tetragonal symmetry structure. Each sample’s mass density was observed to alter as the lead oxide content rose. Scanning electron microscope (SEM) images of the three phases revealed that different Ca-O and Cu-O layers can cause different grain sizes, characterized by elongated thin grains, without a preferred orientation.

목차
1. Introduction
2. Experimental
3. Results and Discussion
4. Conclusions
저자
  • Kareem Ali Jasim(Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad 10001, Iraq)
  • Hind Abdulmajeed Mahdi(Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad 10001, Iraq) Corresponding author
  • Rafah Ismael Noori(Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad 10001, Iraq)
  • Marwa Ayad Abdulmajeed(Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad 10001, Iraq)