In this study, copper oxide, manganese oxide and zeolite, clays containing catalysts were prepared to remove hydrogen sulfide emitted in odor of industry. In order to change the heat treatment temperature, a catalyst was prepared 100 degrees from 600 degrees to 1,000 degrees. GC-MS was used to confirm the hydrogen sulfide removal performance. Although the removal performance produced at 600 degrees was maintained by and large, the removal performance decreased as the temperature increased. In particular, the catalyst manufactured at 900 and 1000 degrees had low removal performance. To find out the cause of the decrease in removal performance, the analytical devices XRD, BET, XRF were used. In order to confirm the properties of the catalyst before and after adsorption, SEM-EDS and CS were used. As a result of analyzing the Cu-Mn catalyst, it was confirmed that the material was adsorbed on the surface. To confirm the adsorbent material, SEM-Mapping was employed. And it was verified that the sulfur was adsorbed. Measuring the SEM-EDS 3Point, it was confirmed to be about 25.09%. Another test method CS analyzer (Carbon/Sulfur Detector) was also deployed. As a result of the test, sulfur was confirmed to be about 27.2%. So comparing the two sets of data, it was verified that sulfur was adsorbed on the surface.