In this study, the refinement of Multiwalled Carbon Nanotubes (MWCNTs) derived from chemical vapor decomposition is investigated. An ultrasonic pretreatment method is employed to disentangle carbon and metal impurities intertwined with MWCNTs. The pretreated MWCNTs exhibit a marginal decrease in C–O/C = O content from 8.9 to 8.8%, accompanied by a 2.5% increase in sp3 carbon content, indicating a mildly destructive pretreatment approach. Subsequently, selective oxidation by CO2 and hydrochloric acid etching are utilized to selectively remove carbon impurities and residual metal, respectively. The resulting yield of intact MWCNTs is approximately 85.65 wt.%, signifying a 19.91% enhancement in the one-way yield of pristine MWCNTs. Notably, the residual metal content experiences a substantial reduction from 9.95 ± 2.42 wt.% to 1.34 ± 0.06 wt.%, representing a 15.68% increase in the removal rate. These compelling findings highlight the potential of employing a mild purification process for MWCNTs production, demonstrating promising application prospects.
Many automotive components for power generation such as motors and alternators have been widely using ferrite magnets. To ensure a high level of efficiency could be achieved in an alternator, the assembled magnets must be in good enough durability. Recently, some hairline cracks have been found on the magnet produced by manufacturers in Korea. Thus, there is an increasing concern that some of the magnets produced could cause further problems after being assembled in the alternator. Based on the standard alternator test (RS0008 : 2006), this paper has developed an accelerated failure-free test for magnets in alternator to demonstrate that assembled magnets will meet durability objective specified by the manufacturer. This guarantees the target life of the magnet with 90 percent reliability and 90 percent confidence level (R90C90). Temperature and rotation speed were selected as accelerated stress factors.