This study was performed to analysis the concentration of TVOC, 5VOC and formaldehyde for building material of total 262 using 20L test chamber. The concentration of TVOC, 5VOC and formaldehyde were measured 1.001㎎/㎡･h, 43.032㎍/㎡･h, 0.012㎎/㎡･h, respectively. TVOC concentration of paint and floor covering occupied the largest concentration of the indoor building materials as 2.689㎎/㎡･h, 2.120㎎/㎡･h, respectively. 5VOC concentration of floor covering was measured 106.636㎍/㎡･h. Toulene and xylene were occupied the largest part of the 5VOC as 51.2% and 33.1%, respectively. The concentration of formaldehyde for furniture materials occupied the largest concentration of the indoor building material as 0.072㎎/㎡h.