The effect of Al(OH)3 on physical, thermal, and retardant property of rubber was studied. It was analyzed by statistical experimental design method with one way array to confirm the effect of factors. Physical characteristics, thermal pyrolysis temperature, and combustion time were considered as the properties. The amount of Al(OH)3 addition was chosen as significant parameter. As the result of ANOVA analysis, thermal pyrolysis temperature increased and combustion time decreased with increasing of Al(OH)3.