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Synthesis and Properties of Glucamine Derivatives with New Composition

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  • URLhttps://db.koreascholar.com/Article/Detail/257288
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한국응용과학기술학회지 (The Korean Society of Applied Science and Technology)
한국응용과학기술학회(구 한국유화학회) (The Korean Society of Applied Science and Technology (KSAST))
초록

The synthesis of N-methyl glucamine was performed in two step reaction. The first step involves the amination between methylamine and glucose in methane. The N-methyl glucamine was obtained by the reduction of using Ni catalyst under the high pressure. The second step was glucamide anionic derivatives synthesis from N-methyl glucamine, maleic anhydride, lauryl alcohol and laurylamine by Schotten Banmann reaction respectively. Their molecular structures of N-methyl glucamine and glucamide (EG-MAS and AC-MAS) were investigated by IR and 1H-NMR. Basic physical properties and biodegradability of there glucamide anionic surfactant was investigated. The range of cmc values determined by measurements of surface tention was 10-5~10-4mol/l and the surface tension of the aqueous solution revealed in the range 28~30 dyne/cm and their biodegradability was very good in the pH 5~10.

저자
  • 박선영 | Park, Seon-Young
  • 김명수 | Kim, Tae-Young
  • 정환경 | Jeong, Hwan-Kyeong
  • 남기대 | Nam, Ki-Dae