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Effect of Reaction Parameters on Silica Nanoparticles Synthesized by Sol-gel Method

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  • URLhttps://db.koreascholar.com/Article/Detail/321916
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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

The sol-gel method is the simplest method for synthesizing monodispersed silica particles. The purpose of this study is to synthesize uniform, monodisperse spherical silica nanoparticles using tetraethylorthosilicate (TEOS) as the silica precursor, ethanol, and deionized water in the presence of ammonia as a catalyst. The reaction time and temperature and the concentration of the reactants are controlled to investigate the effect of the reaction parameters on the size of the synthesized particles. The size and morphology of the obtained silica particles are investigated using transmission electron microscopy and particle size analysis. The results show that monodispersed silica particles over a size range of 54-504 nm are successfully synthesized by the sol-gel method without using any additional process. The nanosized silica particles can be synthesized at higher TEOS/H2O ratios, lower ammonia concentrations, and especially, higher reaction temperatures.

저자
  • 임영현(부산대학교 재료공학부) | Young-Hyun Lim
  • 김도경(건양대학교 의과학과) | Do Kyung Kim
  • 정영근(부산대학교 융합학부) | Young-Keun Jeong Corresponding Author