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나노 크기의 Gd2O3:Eu3+ 적색형광체가 코팅된 판상 Mica의 제조 및 형광특성 KCI 등재

Preparation of Nanosized Gd2O3:Eu3+ Red Phosphor Coated on Mica Flake and Its Luminescent Property

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한국분말야금학회지 (Journal of Korean Powder Metallurgy Institute)
한국분말재료학회(구 한국분말야금학회) (Korean Powder Metallurgy Institute)
초록

Nanosized Gd2O3:Eu3+ red phosphor is prepared using a template method from metal salt impregnated into a crystalline cellulose and is dispersed using a bead mill wet process. The driving force of the surface coating between Gd2O3:Eu3+ and mica is induced by the Coulomb force. The red phosphor nanosol is effectively coated on mica flakes by the electrostatic interaction between positively charged Gd2O3:Eu3+ and negatively charged mica above pH 6. To prepare Gd2O3:Eu3+-coated mica (Gd2O3:Eu/mica), the coating conditions are optimized, including the stirring temperature, pH, calcination temperature, and coating amount (wt%) of Gd2O3:Eu3+. In spite of the low luminescence of the Gd2O3:Eu/mica, the luminescent property is recovered after calcination above 600℃ and is enhanced by increasing the Gd2O3:Eu3+ coating amount. The Gd2O3:Eu/mica is characterized using X-ray diffraction, field emission scanning electron microscopy, zeta potential measurements, and fluorescence spectrometer analysis.

목차
서 론
 2. 실험 방법
  2.1. Gd2O3:Eu3+ 적색형광체의 나노 크기 분산졸 제조
  2.2. Gd2O3:Eu3+가 코팅된 Mica 적색형광체의 제조
  2.3. Gd2O3:Eu/Mica 적색형광체의 특성 분석
 3. 실험결과 및 고찰
  3.1. pH 영향에 따른 Gd2O3:Eu/Mica 적색형광체 제조
  3.2. 온도의 영향에 따른 Gd2O3:Eu/Mica 적색형광체 제조
  3.3. 코팅함량에 따른 Gd2O3:Eu/Mica 적색형광체 제조
 4. 결 론
 감사의 글
 References
저자
  • 김대성(한국세라믹기술원 에코복합소재센터) | Dae-Sung Kim Corresponding Author
  • 반세민(한국세라믹기술원 에코복합소재센터, 부산대학교 융합학부) | Se-Min Ban
  • 박정민(한국세라믹기술원 에코복합소재센터) | Jeong Min Park
  • 정경열(공주대학교) | Kyeong Youl Jung
  • 최병기(㈜씨큐브) | Byung-Ki Choi
  • 강광중(㈜씨큐브) | Kwang-Jung Kang
  • 강명창(부산대학교 융합학부) | Myung Chang Kang