This study was performed to evaluate the odor occurrence of offensive leather odor in a district in Gyeonggi-do, where Jeil industrial complex is located, and its residential district, by using olfactory field frequency measurement (Gird Method). In addition, we measured the composite odor. The target points were 9 spots in Jeil industrial complex and 12 spots in the residential district, and we conducted the measurements 13 times each spot. As a result, odor occurrence in descending order was investigated as follows, leather industry > drug industry > food industry. Moreover, odor exposure of the industrial complex exceeded the industrial zone standard of 0.15 (=German odor standard) in all 9 spots (average 0.78). In addition, odor exposure of the residential district exceeded the residential zone standard of 0.10 (=German odor standard) in 12 spots (average 0.78). All the composite odors were below 20 (industrial zone standard). However, as the odor intensity of the sampling site and the lab analysis data showed a large deviation, we found that much supplementation is needed of the odor analysis techniques in the equipment measurement methods.